Polyester
A polyester and polymer polyester technology, applied in the polyester field, can solve problems such as warming and threatening human existence
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0029] A mixed slurry of 9.2 kg of biological source 1,2-butanediol and 11.3 kg of terephthalic acid was put into the device with a stirring and rectifying tower, and 6.3 g of butyl stannic acid and 6.8 g of tetrabutyl titanate were added. , Gradually increase the temperature to 200-235℃ to carry out the esterification reaction, and collect the by-product water; but when the esterification reaction rate is above 95%, the esterification reaction is ended. After adding 2.6 grams of phosphoric acid, 6.8 grams of titanate is added. Butyl ester, the polycondensation reaction is carried out in the range of 230-250 ℃, when the set polymer viscosity torque is reached, the polymer is discharged and pelletized for use.
Embodiment 2
[0031] The same as the device of Example 1, put in 13.4 kg of dimethyl terephthalate and 11.6 kg of biologically sourced 1,2-butanediol raw materials, add 6 g of cobalt acetate, and carry out the process in the temperature range of 200-235°C After the transesterification reaction, methanol is removed, and the transesterification reaction rate reaches more than 95%, after adding 2.6 grams of phosphoric acid, 6.8 grams of tetrabutyl titanate is added, and the polycondensation reaction is carried out at a temperature of 230-250°C to reach the set polymerization. After the viscosity of the material is reached, spit out the polymer and cut into pellets for later use.
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More