Resin special for paints resistant to strong corrosion and preparation method thereof
A technology of resin and paint, which is applied in the field of special resin for anti-corrosion paint, can solve the problems of atmospheric ozone layer hazard, environmental protection impact, serious problems, etc., and achieve the effect of strong cathodic protection, excellent anti-corrosion performance and less pores
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specific Embodiment 1
[0023] The steps of its specific preparation method are:
[0024] (1) dissolve
[0025] Add pure water into the reactor, start the agitator, slowly put polyvinyl alcohol into the reactor, start heating to 95-99°C, and keep it warm for 4-6 hours to ensure that the polyvinyl alcohol is completely dissolved;
[0026] (2) Reaction
[0027] Lower the temperature of the solution to 30-45°C, slowly add the immobilized heteropolyacid catalyst to the polyvinyl alcohol solution, and stir for 30 minutes; then slowly add butyraldehyde to the solution, and when the amount of butyraldehyde is added to half, slowly add Ethanol, zinc powder, after adding the three materials, stir for 4 hours;
[0028] (3) Dehydration
[0029] The temperature of the solution is lowered to normal temperature, the solution is centrifuged and dehydrated, and the resin generated by the reaction is separated;
[0030] (4) dry
[0031] Dry the resin at a temperature of 55-70° C. so that the moisture contained i...
specific Embodiment 2
[0033] The steps of its specific preparation method are:
[0034] (Add pure water to the reactor, start the agitator, slowly put polyvinyl alcohol into the reactor, start heating to 95-99°C, keep warm for 4-6 hours, to ensure that the polyvinyl alcohol is completely dissolved;
[0035] (2) Reaction
[0036] Lower the temperature of the solution to 30-45°C, slowly add the immobilized heteropolyacid catalyst to the polyvinyl alcohol solution, and stir for 30 minutes; then slowly add butyraldehyde to the solution, and when the amount of butyraldehyde is added to half, slowly add Ethanol, zinc powder, after adding the three materials, stir for 4 hours;
[0037] (3) Dehydration
[0038] The temperature of the solution is lowered to normal temperature, the solution is centrifuged and dehydrated, and the resin generated by the reaction is separated;
[0039] (4) dry
[0040] Dry the resin at a temperature of 55-70° C. so that the moisture contained in the resin reaches 0.1 percen...
specific Embodiment 3
[0042] The steps of its specific preparation method are:
[0043] Add pure water into the reactor, start the agitator, slowly put polyvinyl alcohol into the reactor, start heating to 95-99°C, and keep it warm for 4-6 hours to ensure that the polyvinyl alcohol is completely dissolved;
[0044] (2) Reaction
[0045] Lower the temperature of the solution to 30-45°C, slowly add the immobilized heteropolyacid catalyst to the polyvinyl alcohol solution, and stir for 30 minutes; then slowly add butyraldehyde to the solution, and when the amount of butyraldehyde is added to half, slowly add Ethanol, zinc powder, after adding the three materials, stir for 4 hours;
[0046] (3) Dehydration
[0047] The temperature of the solution is lowered to normal temperature, the solution is centrifuged and dehydrated, and the resin generated by the reaction is separated;
[0048] (4) dry
[0049] Dry the resin at a temperature of 55-70° C. so that the moisture contained in the resin reaches 0.1...
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