Synthesis technology of water-emulsion fluorescent pigment
A technology of fluorescent pigments and synthesis process, applied in the field of fluorescent pigments, can solve the problems of environmental protection, poor fluorescence, high viscosity of water-emulsion fluorescent pigments, etc.
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Embodiment 1
[0016] Table 1: Raw material ratio of fluorescent pigment in embodiment 1
[0017] raw material
weight
weight
Butadiene
62
Emulsifier
9.2
38
0.3
7.2
Initiator
0.2
Deionized water
120
Fluorescent dyes
5.1
[0018] a. Emulsification process: Put deionized water and emulsifier into the emulsification kettle, heat to 60°C and dissolve completely, add reaction monomer butadiene, styrene, acrylic acid and fluorescent dye, stir evenly, and use high-shear emulsification head Emulsified to obtain the emulsion for subsequent use;
[0019] b, seed emulsion synthesis process: take 15% of the total amount of the standby emulsion to synthesize the seed emulsion, pump the 15% emulsion into the reaction kettle with a metering pump, stir, heat to 60-90°C, add an initiator to react, And control the reaction temperature between 60-90°C, and ...
Embodiment 2
[0023] Table 2: Raw material ratio of fluorescent pigment in embodiment 2
[0024] raw material
weight
raw material
weight
55
Emulsifier
8.7
45
0.3
7.9
Initiator
0.2
Deionized water
140
Fluorescent dyes
6.3
[0025] a. Emulsification process: Put deionized water and emulsifier into the emulsification kettle, heat to 50°C and dissolve completely, add reaction monomer methyl methacrylate, butyl methacrylate, acrylic acid and fluorescent dye, stir evenly, and emulsify 2 hours to get the emulsion for later use;
[0026] b, seed emulsion synthesis process: take 5% of the total amount of the standby emulsion to synthesize the seed emulsion, pump the 5% emulsion into the reaction kettle with a metering pump, stir, heat to 60-90°C, add an initiator to react, And control the reaction temperature between 60-90°C, a...
Embodiment 3
[0030] Table 3: Raw material ratio of fluorescent pigment in embodiment 3
[0031] raw material
weight
raw material
weight
67
Emulsifier
9.4
33
0.3
[0032] raw material
weight
raw material
weight
acrylic acid
8.6
Initiator
0.2
Deionized water
130
Fluorescent dyes
7.1
[0033] a. Emulsification process: put deionized water and emulsifier into the emulsification kettle, after heating and dissolving completely, add reaction monomer methyl methacrylate, acrylonitrile, acrylic acid and fluorescent dye, stir evenly, and emulsify to obtain emulsion for later use;
[0034] b, seed emulsion synthesis process: take 20% of the total amount of the standby emulsion to synthesize the seed emulsion, pump 20% of the emulsion into the reaction kettle with a metering pump, stir, heat to 60-90°C, add an initiator ...
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