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Apparatus and process for the production of nanocarbon material

A technology for nano-carbon materials and manufacturing devices, which is applied in the direction of nano-structure manufacturing, nano-technology, nano-technology, etc., and can solve the problem of low yield of carbon materials

Inactive Publication Date: 2011-05-04
MITSUBISHI HEAVY IND LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] However, the production methods disclosed in the above-mentioned documents are all laboratory or small-scale production methods, and there is a problem that the yield of carbon materials is low in particular.

Method used

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  • Apparatus and process for the production of nanocarbon material
  • Apparatus and process for the production of nanocarbon material
  • Apparatus and process for the production of nanocarbon material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment approach 1

[0119] A schematic diagram of a carbon nanomaterial manufacturing device that prevents entanglement of carbon nanofibers by pH adjustment in this embodiment is shown in figure 1 .

[0120] Such as figure 1 As shown, the nano-carbon material manufacturing device 10-1A in the embodiment is equipped with: a nano-carbon material manufacturing unit 15 that utilizes a fluidized bed reactor to manufacture the nano-carbon material 14 with a catalyst; the obtained nano-carbon material 14 with a catalyst is dispersed In the acid solution, the fluidized catalyst 12 as the granulation catalyst is dissolved and separated with the acid solution 21; the washing part 22 is arranged on the downstream side of the acid treatment part 21, and the nano-carbon material after the acid treatment is washed with water; Be arranged on the downstream side of the above-mentioned water washing part 22, adjust the pH of the aqueous solution after washing to the weak base side with a medicament; the dryin...

Embodiment approach 2

[0178] In this embodiment, the schematic diagram of the nano-carbon material manufacturing device for adding oxygen-containing functional groups is shown in Figure 6 . Figure 7 is a schematic diagram showing the behavior of nanocarbons caused by the repulsion of oxygen-containing functional groups. It should be noted that, for figure 1 The same configurations of the shown apparatuses according to the first embodiment are denoted by the same symbols, and descriptions thereof are omitted (the same applies hereinafter).

[0179] Such as Figure 6 As shown, the nano-carbon material manufacturing device 10-2A of Embodiment 2 is composed of the following parts: a nano-carbon material manufacturing part 15 that utilizes a fluidized bed reactor 13 to manufacture a nano-carbon material 14 with a catalyst; Oxygen-containing functional group addition treatment section 27 for adding oxygen-containing functional groups to the carbon material 14; dispersing the catalyst-bearing nano-c...

Embodiment approach 3

[0202] The schematic diagram of the nano-carbon material manufacturing device that implements the treatment of replacing with a fast-drying solvent in Embodiment 3 is shown in Figure 12 .

[0203] Such as Figure 12As shown, the nano-carbon material manufacturing device 10-3A of the embodiment is equipped with: a nano-carbon material manufacturing unit 15 that manufactures a nano-carbon material 14 with a catalyst through a fluidized bed reactor 13; and disperses the obtained nano-carbon material 14 with a catalyst. In the acid solution, the fluidized catalyst 12 as the granulation catalyst is dissolved and separated with the acid solution 21; the washing part 22 is arranged on the downstream side of the acid treatment part 21, and the nano-carbon material after the acid treatment is washed with water; Set on the downstream side of the above-mentioned water washing part 22, a quick-drying solvent replacement part 28 replaced with a quick-drying solvent; and a drying part 24 ...

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Abstract

Included are a nano-carbon material production unit (15) for producing a nano-carbon material using a fluidized catalyst (12) formed by granulating a carrier supporting an active component, an acid treatment unit (21) for dissolving and separating a catalyst by an acid solution by feeding a catalyst-containing nano-carbon material (14) into the acid solution, and a pH adjustment unit (23), which is an anti-agglomeration treatment unit, provided on a downstream side of the acid treatment unit (21), for performing an anti-agglomeration treatment to prevent agglomeration among nano-carbons due to repulsion caused by dissociation among oxygen-containing functional groups added to the nano-carbon material.

Description

technical field [0001] The present invention relates to a nanocarbon material production device and a nanocarbon production method that increase the yield of an effective nanocarbon material. Background technique [0002] A carbon nanotube is a tubular carbon polyhedron having a structure in which graphite sheets are closed in a cylindrical shape. The carbon nanotube includes: a multilayer nanotube with a multi-layer structure in which graphite sheets are closed into a cylinder, and a single-layer nanotube with a single-layer structure in which graphite sheets are closed into a cylinder. [0003] The multilayered nanotubes were discovered by Iijima in 1991. That is, it was found that multilayered nanotubes exist in a carbon block deposited on the cathode of the arc discharge method (Non-Patent Document 1). Then, research on multilayer nanotubes has been actively carried out, and in recent years it has been possible to synthesize multilayer nanotubes in large quantities. ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B31/02
CPCB01J8/005B01J8/1836B01J2208/00592B01J2208/00681B01J2219/00006B82Y30/00B82Y40/00C01B32/162B82B3/0004
Inventor 龙原洁杉山友章田中敦濑户口稔彦
Owner MITSUBISHI HEAVY IND LTD
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