Method for detecting sludge cell wall breakage
A sludge and cell technology, which is applied in the direction of weighing by removing a certain component, analyzing the material by observing the influence on the chemical indicator, and analyzing by chemical reaction of the material, etc. It can solve the problem of high equipment requirements and reliability. Problems such as poor sexuality and insignificant indicative effect
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[0076] 1. Measure the original TCOD
[0077] Take 1.00ml of the remaining sludge as it is, dilute 20 times with distilled water, put it in a 500mL conical flask, add 10ml of potassium dichromate to it, add water to dilute to 110mL±1, and slowly add 30mL of concentrated sulfuric acid, shake well, Heat to reflux in a strong acidic medium for 2 hours; after cooling, rinse the wall of the condenser tube with 90.00ml of water, remove the Erlenmeyer flask; then add 3 drops of test ferrousin indicator solution (about 0.14-0.16mL) mol / L ammonium ferrous sulfate standard solution titration, the color of the solution is from yellow to blue-green to reddish brown as the end point, record the amount of ammonium ferrous sulfate standard solution V 1 = 16ml; take 20.00mL of distilled water, and do a blank experiment according to the same procedure. Record the consumption V of ferrous ammonium sulfate standard solution when titrating the blank 0 = 45ml.
[0078] Calculation of TCOD of raw...
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