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Papermaking and pulping method capable of obtaining black liquor at high concentration

A high-concentration, black liquor technology, applied in the direction of pulping with inorganic alkali, can solve the problem of low black liquor concentration, and achieve the effect of reducing pollution load and energy consumption

Inactive Publication Date: 2012-06-13
SHANDONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The present invention aims at the problem that the solid-liquid phase residence time is the same in the cooking process of the existing intermittent or continuous alkaline pulping process, and the concentration of the black liquor discharged during the cooking process is low, and provides a black liquor by-product that can be conveniently obtained with a higher concentration, A papermaking pulping method that effectively reduces energy consumption in the subsequent black liquor concentration process and obtains high-concentration black liquor

Method used

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  • Papermaking and pulping method capable of obtaining black liquor at high concentration
  • Papermaking and pulping method capable of obtaining black liquor at high concentration
  • Papermaking and pulping method capable of obtaining black liquor at high concentration

Examples

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Embodiment 1

[0014] This embodiment adopts the vertical countercurrent cooking process of feeding at the bottom of the cooking tower, such as figure 1 It is shown that the solid phase raw material is fed from the bottom of the digestion tower in this process. The solid phase wood chips or forage raw materials are fed from the bottom of the cooking tower by the raw material feeding system, and the inside of the cooking tower is equipped with a screw elevator, which gradually lifts the solid phase materials entering the cooking tower to the top of the tower, and then is fed by the pulp Material discharge system discharge. The interior of the cooking tower is equipped with distributors for fresh water, evaporative condensed water (from MVR) and concentrated lye, and the above water or solution is pumped into the tower, sequentially from the top to different positions. The evaporative condensed water produced during the concentration process of black liquor by mechanical vapor recompression i...

Embodiment 2

[0016] This embodiment adopts the overall countercurrent single digester parallel flow process, such as figure 2 Show. Single parallel flow of digesters is a more common pulping method at present. According to the theory of fluid plug flow and full mixed flow mode, combined with the back-mixing situation in actual flow operation, a single digester in multi-stage series can be used for continuous operation, which can also achieve approximate The operation effect of push flow. Therefore, in this embodiment, slurry washing, concentrated alkali liquor cooking and black liquor precooking are connected in series to achieve the purpose of overall countercurrent continuous operation. A solid-liquid separator and a material conveying system are installed between each single digester to form a countercurrent continuous operation system. In order to achieve a better washing effect, the slurry washing with black liquor after cooking can also be operated in the same single-stage paralle...

Embodiment 3

[0018] This embodiment adopts the vertical countercurrent cooking process of feeding at the top of the cooking tower, such as image 3 As shown, the solid phase material is fed from the top of the digestion tower in this process. Solid-phase wood chips or forage raw materials are fed from the top of the cooking tower by the raw material feeding system, and there is no screw elevator inside the cooking tower. The solid phase material entering the tower moves to the bottom of the tower through settling, and a pulp discharge system is installed at the bottom of the tower. Distributors for fresh water, steam condensed water and concentrated lye are still installed inside the cooking tower. Fresh water, evaporative condensed water generated during the concentration process, and concentrated lye are pumped into different sections of the tower from different positions downward from the top of the tower. the distributor. Adjust the liquid ratio in the cooking device to be 3-5:1, and...

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Abstract

The invention provides a papermaking and pulping method capable of obtaining black liquor at high concentration. In a digester, the inlet direction of a solid phase raw material is reverse to that of a concentrated alkali solution; at least two concentrated alkali solution distributors with different heights are arranged in the digester; a heating device is arranged on the outer side or the innerside of the digester; the evaporative condensate water which is produced in the concentration process of the black liquor is used as water for dilution of the concentrated alkali solution; slurry is washed by the reverse flow of fresh water and the slurry; the liquor ratio in the digester is adjusted to be (3-5):1; and the effective alkali concentration gradient is 90 to 6g / L. A countercurrent continuous digestion process is adopted; different residence time of solid and liquid phases in a digestion process is reasonably adjusted; the reasonable liquor ratio is guaranteed, the effective alkali content in the back liquor is controlled; the slurry is subjected to countercurrent washing by using fresh make-up water and high-temperature condensate water which is generated in the concentrationprocess of the back liquor, so the amount of water used in the digestion process can be reduced by 70 to 80 percent; the solid content of the back liquor can reach over 20 percent; and the power consumption of black liquor concentration is reduced by over 50 percent.

Description

technical field [0001] The invention relates to a papermaking and pulping method capable of obtaining high-concentration black liquor, and belongs to the interdisciplinary technical field of biomass energy and papermaking and pulping. Background technique [0002] The paper industry is well-known as a major water resource consumer and water polluter. The key to the problem is that the black liquor in pulping wastewater is difficult to biodegrade. In particular, the wood pulp black liquor concentration, incineration power generation, and alkali recovery treatment processes imitated to control straw pulp black liquor pollution are still not perfect and need further improvement. Among them, the concentration process requires a lot of energy consumption, which consumes the meager profits of the straw pulp pulping process, and also greatly increases the cost of the straw pulp production process, making it gradually lose its commercial competitiveness. Ultimately, most straw pulp...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D21C3/02
Inventor 苏继新刘思明孙越吕刚林李群张志轩
Owner SHANDONG UNIV
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