Method for growing nitride light emitting diode by adopting metal-organic chemical vapor deposition (MOCVD) technology
A technology of light-emitting diodes and nitrides, applied in gaseous chemical plating, coatings, electrical components, etc., can solve the problems of poor electrical parameters such as leakage and antistatic, and unsatisfactory effects
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[0019] The invention relates to a method for growing gallium nitride epitaxy on a pattern substrate. Using MOCVD technology, using high-purity NH 3 As N source, high-purity N 2 or H 2 As carrier gas, trimethylgallium (TMGa) or triethylgallium (TEGa), trimethylindium (TMIn) and trimethylaluminum (TMAl) are respectively used as gallium source, indium source and aluminum source; silane (SiH 4 ) is an N-type dopant, magnesium dicene (CP 2 Mg) is a P-type dopant. Such as figure 2 As shown, at first, in the MOCVD reaction chamber, pattern substrate 21 is subjected to heat treatment: in H 2 Under the atmosphere, the temperature is maintained at 1100-1180°C, and the baking is continued for 600-2000 seconds; then, the temperature and pressure of the reaction chamber are adjusted: the temperature is 510-570°C, the pressure is 400mbar-800mbar, and the metal source and NH 3 , grow a nitride nucleation layer, when the thickness of the nucleation layer reaches 20-50nm, stop feeding t...
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