Disperse dye composition, dye product and application thereof
A technology of disperse dyes and compositions, applied in organic dyes, dyeing methods, textiles and papermaking, etc.
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[0096] Example 1
[0097] 35.0 g of the original dye represented by formula (1-1), 2.4 g of original dye represented by formula (1-2), 1.8 g of original dye represented by formula (2-5), and formula (2-7) 10.8 g of the original dye shown, 70 g of the dispersant MF, and 200 g of pure water are used together with a sand mill for micronization (for dispersion treatment), and then spray-dried to obtain a yellow-brown disperse dye composition. Based on the original dye used, the mass fraction of component A represented by formula (1-1) and formula (1-2) is 74.8%, and the mass fraction of component B represented by formula (2-5) and formula (2-7) Is 25.2%.
[0098] The double-layer filter paper filtration method was used to test the dispersion stability of the disperse dye of the present invention at 71°C and 130°C according to GB / T 5540 and GB / T 5541-2007, respectively. Among them, the "residue" level at 71°C is level 4, and the "filtration time" level is level A; the "residue" level ...
Example
[0105] Examples 2-20
[0106] According to the data shown in Table 1, Component A, Component B, Component C, Component D, Component E, Component F, 70 grams of dispersant MF and 200 grams of water were ground and dispersed together with a sand mill And then spray-dried to produce disperse dyes.
[0107] Table 1 :
[0108]
Example Embodiment
[0109] Example 21
[0110] Take 0.25 g of the disperse dyes prepared in Examples 1-20 (owf=5%) and 0.075 g of glacial acetic acid (1g / l) to make 75 ml of dye solution, and put in 5.0 g of polyester superfine fiber and spandex (12%). ) Blended fabric (commonly known as T+OP cloth, the grey fabric is pre-formed and refined at 180~195℃). The fabric is dyed from room temperature to 130℃ within 60 minutes, kept for 45 minutes, and cooled to below 85℃. Treat the fabric with sodium dithionite and sodium hydroxide at 85°C for 20 minutes, and then treat the fabric with an acid reducing agent (such as hydroxyalkyl sulfinate) at a pH of 3.5 to 5.0 at 85°C for 20 minutes, and rinse with water. Dry, dry heat and set at 160°C for 30 seconds to obtain a deeply colored fabric.
[0111] Respectively according to the 2A method specified in AATCC 61-2007 home and commercial washing color fastness, GB / T5713-1997 textile color fastness test water fastness (equivalent to ISO 105-E01), GB / T5718-1997 te...
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