Method for evaluating aging degree of crosslinked polyethylene cable based on nuclear magnetic resonance
A cross-linked polyethylene, nuclear magnetic resonance technology, applied in the direction of analysis by nuclear magnetic resonance, can solve the problems of aging factors, aging, differences and other problems that cannot be fully considered
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[0029] The method of the present invention refers to the following steps.
[0030] 1) Using nuclear magnetic resonance to obtain the molecular structure of normal XLPE cables
[0031] Take the insulating layer material (cross-linked polyethylene) of the normal (new factory) cable sample, sample along the axial direction of the insulating layer, cut into particles of uniform size, and weigh 1.2g as a normal sample.
[0032] The normal sample is analyzed by nuclear magnetic resonance analyzer. The parameters of nuclear magnetic resonance analyzer are set as follows: the center frequency (SF1) is 22MHz, the offset frequency (O1) is 584.347825 KHz, the pulse sequence repetition time (TR) is 2000us, and the number of repeated sampling (NS) is 16, attached figure 2 is the NMR inversion spectrum of the sample obtained under this parameter setting.
[0033] Obtain the peak area SP of normal XLPE cables by NMR analysis 0 and the longitudinal relaxation time RTL 0 , the peak area S...
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