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98 results about "Longitudinal Relaxation Time" patented technology

Method for measuring atomic transverse relaxation time based on electron resonance phase frequency analysis

InactiveCN106597338ASuppression of the effects of common coefficient fluctuationsExact transverse relaxation timeMeasurements using electron paramagnetic resonanceAnalysis using electron paramagnetic resonanaceFrequency spectrumTransverse magnetic field
The invention discloses a method for measuring atomic transverse relaxation time based on an electron resonance phase frequency analysis. In a strong-background magnetic field with almost neglected residual magnetization in a magnetic shielding barrel, a swept-frequency signal that has a bandwidth covering a resonance curve and has an amplitude enabling the resonance curve to have a clear curve under low polarizability is applied in a horizontal direction; an optical swing angle signal of a magnetometer is detected and a spectral analysis is carried out on an outputted signal in a polar coordinate system to obtain a phase frequency response function of the magnetometer; the phase frequency response function is fitted to a corresponding theoretical phase frequency curve of the magnetometer to obtain atomic spinning transverse relaxation time. Because the phase angle is a result obtained by quotient processing of a spinning transverse component, the influence of common coefficient fluctuation is suppressed, so that the phase frequency signal expression is more stable by being compared with amplitude-frequency signal expression. Besides, the theoretical phase frequency curve is not affected by the magnetic induction intensity of the transverse magnetic field and the atomic spinning longitudinal relaxation time, so that complexity of data processing can be reduced. Moreover, a lorenz curve widening risk caused by the transverse magnetic field can be eliminated.
Owner:BEIHANG UNIV

Petroleum reservoir rock constituent identification and quantitative evaluation method

The invention provides a petroleum reservoir rock constituent identification and quantitative evaluation method. The method comprises the steps that nuclear magnetic resonance response signals of sample rocks are received, and inversion is performed on the response signals so that a first spectrogram is acquired; aperiodic relaxation time T2sec and the specific value T1/T2 of longitudinal relaxation time T1 to transverse relaxation time T2 are calculated according to the first spectrogram, and the first spectrogram is projected to a coordinate system with the specific value T1/T2 of longitudinal relaxation time T1 to transverse relaxation time T2 and aperiodic relaxation time T2sec acting as coordinate axes so that a second spectrogram is formed; and locating areas of different hole types are divided on the second spectrogram according to the preset cut-off value, and the proportion of each hole type is obtained via an integration method. According to the petroleum reservoir rock constituent identification and quantitative evaluation method, accuracy of reservoir rock constituent identification and reliability of the reservoir quantitative evaluation result can be enhanced.
Owner:CHINA UNIV OF PETROLEUM (BEIJING)

Magnetic-resonance imaging method for synchronous measurement of fluid speed and temperature in porous medium

ActiveCN103776490ANo optical requirementsCompensate for temperature deficienciesMeasurement devicesNMR - Nuclear magnetic resonancePorous medium
Disclosed is a magnetic-resonance imaging method for synchronous measurement of fluid speed and temperature in a porous medium and the method belongs to the field of magnetic-resonance imaging measurement. The method adopts a nuclear-magnetic-resonance overturning restoring label method: firstly a spin-echo sequence two-point method is used to measure a longitudinal relaxation time T1 of a tested fluid at a specific temperature; step 1 is repeated at different temperatures so that T1 values at different temperatures are obtained and then the relation between T1 and temperature T is obtained through fitting; an overturning restoring label sequence is used to measure the fluid at a static state and then the fluid at any temperature and flow speed is measured; a matlab is used to read an image so that image signal intensity (SI) distribution is obtained, and then the temperature T is calculated according to the relation of SI and T; label displacement within an overturning restoring time ti is solved through comparison of a label coordinate under the flow speed and a label coordinate at a static state so that a fluid flow speed is solved. The magnetic-resonance imaging method for the synchronous measurement of the fluid speed and the temperature in the porous medium is high in measurement speed and capable of compensating effectively for signal reduction resulted from flowing when a traditional overturning restoring method is used to measure flow-field temperatures.
Owner:DALIAN UNIV OF TECH

pH value testing method

The invention relates to the field of biological medicines, in particular to a pH value testing method which comprises the following steps: with an amino proton as an endogenous contrast agent, testing corresponding chemical exchange saturated transferring effect ratios R of amino protons of known pH value amino proton source solutions under different saturated pulse intensities, establishing function relationships of pH values and the ratios R corresponding to the different known pH value amino proton source solutions according to the different known pH value amino proton source solutions andtested corresponding ratios R, and finally calculating expected pH values according to the function relationships of values Ri tested through experiments and the function relationships. By adopting the method, influence of concentrations can be eliminated, parameters such as exchangeable proton concentrations and longitudinal relaxation times of water do not need to be estimated or measured, so that pH values can be relatively accurately, conveniently and non-destructively measured. In addition, since amino is relatively low in chemical exchange velocity, stable imaging under magnetic resonance field intensity of common clinical application can be achieved, and thus the method has good application prospects.
Owner:SHENZHEN INST OF ADVANCED TECH

Method for determining conversion rate during p-polyisobutylene phenol synthesis process through quantitative nuclear magnetic resonance spectroscopy

ActiveCN108152318AAvoid cumbersomeImprove accuracyAnalysis using nuclear magnetic resonanceTwo-dimensional nuclear magnetic resonance spectroscopyPhenol
The invention relates to a method for determining the conversion rate of polyisobutylene, in particular to a method for determining the conversion rate of the polyisobutylene during a process of generating p-polyisobutylene phenol through reaction of the polyisobutylene and excessive phenol through a quantitative nuclear magnetic resonance spectroscopy. The method comprises the steps of respectively acquiring a polyisobutylene phenol sample, and a polyisobutylene and phenol nuclear magnetic resonance spectroscopy, obtaining chemical shift of the p-polyisobutylene phenol through spectrogram comparison and spectrogram reasoning; determining longitudinal relaxation time T1 of a p-polyisobutylene phenol sample in a deuteration reagent, setting a pulse flip angle and relaxation time of a nuclear magnetic resonance spectrometer according to the T1, utilizing the nuclear magnetic resonance spectrometer for determining the nuclear magnetic resonance spectroscopy of a solution to be tested, obtaining a peak area of each part of hydrogen through integration, and calculating to obtain the conversion rate of the polyisobutylene through the number of hydrogen actually contained in a target product and raw materials. The method provided by the invention is low in cost, can be used for quickly and accurately evaluating the type and the conversion rate of a synthetic product of the polyisobutylene and the phenol, and provides a powerful evidence for synthesis.
Owner:CHAMBROAD CHEM IND RES INST CO LTD

Measuring method and device for underground thick oil molecule chain length

The invention provides a measuring method and device for the underground thick oil molecule chain length. The method comprises the steps that a three-dimensional nuclear magnetic resonance pulse sequence is emitted into a probe of a nuclear magnetic resonance fluid analyzer filled with a thick oil sample, wherein the three-dimensional nuclear magnetic resonance pulse sequence contains three independent windows used for editing information of the longitudinal relaxation time T<1>, information of the diffusion coefficient D and information of the transverse relaxation time T<2> respectively; echo data is collected; inversion is performed on the echo data by adopting a fast inversion algorithm, and a joint probability distribution function about the longitudinal relaxation time T<1>, the diffusion coefficient D and the transverse relaxation time T<2> is calculated; a probability distribution function of the molecule chain length of all components in the thick oil sample is solved according to a pre-established model of the relation between the longitudinal relaxation time T<1> and the molecule chain length of all the components in the thick oil sample or a pre-established model of the relation between the diffusion coefficient D and the molecule chain length of all the components in the thick oil sample or a pre-established model of the relation between the transverse relaxation time T<2> and the molecule chain length of all the components in the thick oil sample.
Owner:CHINA UNIV OF PETROLEUM (BEIJING)
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