The invention provides a method for obtaining a high-resolution two-dimensional J 
decomposition spectrum, and relates to a 
nuclear magnetic resonance spectroscopy detection method. The method comprises: loading a sample to be detected into a standard nuclear magnetic 
test tube, and conveying into the detection chamber of a 
nuclear magnetic resonance spectrometer; sampling the one-dimensional 
hydrogen spectrum of the sample to be detected, and obtaining the 
signal peak distribution area and the 
spectral line width so as to provide the reference for the 
spectral width parameter setting, wherein the 
line width value reflects the 
magnetic field uniformity condition; measuring the pulse width of a 
radio frequency pulse required by excitation of the sample to be detected; introducing a compiled 
pulse sequence on the 
nuclear magnetic resonance spectrometer, opening the heteronuclear intermolecule 
multiple quantum coherent 
signal excitation module, the indirect dimensional evolving module, the 
spin echo fixed 
delay module and the J modulating fast sampling module of the 
pulse sequence, and setting the experiment parameters of various modules; skipping the artificial shimming operation process, and directly executing data sampling; and after completing the data sampling, calling data post-
processing codes to carry out related data post-
processing so as to obtain the high-resolution two-dimensional J 
decomposition spectrum being not affected by the inhomogeneous 
magnetic field.