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Manufacturing method of electrode foil for high voltage aluminum electrolytic capacitor

A technology for aluminum electrolytic capacitors and manufacturing methods, which is applied to electrolytic capacitors, capacitors, circuits, etc., can solve problems such as low production efficiency and poor storage performance, and achieve the effects of high production efficiency, improved density, and improved manufacturing efficiency

Active Publication Date: 2016-03-30
内蒙古丰川电子科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This electrode foil manufacturing method has low production efficiency and poor storage performance

Method used

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  • Manufacturing method of electrode foil for high voltage aluminum electrolytic capacitor

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0010] Example 1, first immerse the corroded foil in pure water at 95°C for 10 minutes, then take it out and place it in an aqueous solution of 0.1% adipic acid and 0.1% adipic acid salt, and then at 75°C with a current density of 20mA / cm 2 , Under the condition of a voltage of 160V, carry out the primary formation for 10 minutes; take out the corroded foil after the primary formation, and then place it in an aqueous solution of 0.1% adipic acid and 0.1% adipic acid salt, and then heat it at 75°C , the current density is 20mA / cm 2 , under the condition of 320V voltage, carry out the secondary formation for 10 minutes; take out the corroded foil after the secondary formation, rinse it with water, put it in the aqueous solution of 0.1% azelaic acid and 0.1% azelaic acid salt, and then put it in 75 ℃, the current density is 20mA / cm 2 , Under the condition of a voltage of 460V, the tertiary formation was carried out for 10 minutes; the corroded foil after the tertiary formation...

Embodiment 2

[0011] Example 2, first immerse the corroded foil in pure water at 98°C for 5 minutes, then take it out and place it in an aqueous solution of 5% adipic acid and 5% adipic acid salt, and then at 90°C with a current density of 20mA / cm 2 , Under the condition of a voltage of 160V, carry out the primary formation for 8 minutes; take out the corroded foil after the primary formation, and then place it in an aqueous solution of 5% adipic acid and 5% adipic acid salt, and then heat it at 90°C , the current density is 20mA / cm 2 1. Under the condition of 320V voltage, carry out secondary formation for 8 minutes; take out the corroded foil after secondary formation, rinse it with water, put it in an aqueous solution of 2% azelaic acid and 2% azelaic acid salt, and then put it in 90 ℃, the current density is 20mA / cm 2 , Under the condition of a voltage of 460V, the three-stage formation was carried out for 8 minutes; the corroded foil after the three-stage formation was placed in an ...

Embodiment 3

[0012] Example 3, first immerse the corroded foil in pure water at 90°C for 10 minutes, then take it out and place it in an aqueous solution of 4% adipic acid and 4% adipic acid salt, and then heat it at 85°C with a current density of 20mA / cm 2 , Under the condition of a voltage of 160V, carry out primary formation for 10 minutes; take out the corroded foil after primary formation, and then place it in an aqueous solution of 4% adipic acid and 4% adipic acid salt, and then heat it at 85°C , the current density is 20mA / cm 2 , under the condition of 320V voltage, carry out the secondary formation for 10 minutes; take out the corroded foil after the secondary formation, rinse it with water, put it in the aqueous solution of 2% azelaic acid and 1% azelaic acid salt, and then put it in 85 ℃, the current density is 20mA / cm 2 , Under the condition of a voltage of 460V, the tertiary formation was carried out for 10 minutes; the corroded foil after the tertiary formation was placed ...

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Abstract

The invention discloses a five-stage manufacturing method of an electrode foil for a high-voltage aluminium electrolytic capacitor. The five-stage manufacturing method comprises the following steps of: (A) firstly putting a corroded foil in pure water for impregnation, then taking out the corroded foil, and then putting the corroded foil in aqueous solution with adipic acid and adipic acid salt to carry out first-stage formation; (B) after taking out the foil, putting the foil in the aqueous solution with the adipic acid and the adipic acid salt again to carry out second-stage formation; (C) after taking out the foil, using water to wash the foil, and then putting the foil in aqueous solution with azelaic acid and azelaic acid salt to carry out third-stage formation; (D) then putting the foil in the aqueous solution with the azelaic acid and the azelaic acid salt again to carry out fourth-stage formation, and then carrying out high temperature thermal treatment after the fourth-stage formation ; and (E) then putting the foil in the aqueous solution with the azelaic acid and the azelaic acid salt again to carry out fifth-stage formation; then carrying out polarization treatment in phosphoric acid solution; and taking out and drying the foil. Compared with the prior art, the five-stage manufacturing method disclosed by the invention has the advantages of high production efficiency and good storage performance.

Description

technical field [0001] The invention relates to a manufacturing method of an electrode foil for a capacitor, and is especially suitable for a five-stage manufacturing method of the electrode foil for a high-voltage aluminum electrolytic capacitor. Background technique [0002] Prior to this, the manufacturing method of electrode foil for high-voltage aluminum electrolytic capacitors was as follows: immerse corroded aluminum foil with a purity of 99.99% in pure water at 95-100°C for 10 minutes, then take it out and place it in 5% in an aqueous solution of boric acid and 0.1% fumaric acid, and then at 85°C with a current density of 20mA / cm 2 , Under the condition of a voltage of 280V, carry out primary synthesis for 18 minutes; then place it in an aqueous solution of 5% boric acid and 0.1% fumaric acid, at 85°C, the current density is 20mA / cm 2 , Under the condition of a voltage of 550V, secondary formation for 18 minutes; then placed in an aqueous solution of 5% boric acid a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01G9/055
Inventor 杨富国张玉红
Owner 内蒙古丰川电子科技有限公司