Improvement of potassium nitrate producing method

A production method, the technology of potassium nitrate, applied in the direction of preparation of alkali metal nitrate, etc., can solve the problems of difficult separation, difficulty in simplifying the production process, and high operation requirements, and achieve the effects of reducing consumption, considerable economic benefits, and reducing fuel consumption

Inactive Publication Date: 2013-08-21
朱建江
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These two methods inevitably have the characteristics of difficult separation, hi

Method used

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Experimental program
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Effect test

Embodiment approach 1

[0029] Embodiment 1: The present invention is an improvement based on the existing potassium nitrate production method, specifically, it improves the 3rd step and the 10th step of the existing method.

[0030] The production method of potassium nitrate is as follows:

[0031] 1. According to the content of each substance in the circulating mother liquor or clear water, add a certain amount of potassium chloride (a certain amount of ammonium nitrate should be added when using clear water), let the above-mentioned substances mix and react (heating or not);

[0032] 2. a. For the heating reaction, the solution should be cleared or cleared with a filter, and the clear solution should be poured into the crystallizer or pumped into the crystallizer to crystallize (the crystallization is: potassium nitrate, ammonium chloride and other mixture crystallization ). B, directly proceed to the next step for the reaction without heating;

[0033] 3. The solid-liquid mixture is crystallize...

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PUM

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Abstract

The invention relates to a potassium nitrate producing method, and in particular relates to partial improvement of a potassium nitrate producing method. The improvement of the potassium nitrate producing method disclosed by the invention is characterized in that 1) solid-liquid blending is performed on solid-liquid mixture crystals by using clear water, crystal water or washing water by a volume ratio of 10% to 80%, and the liquid can be recycled, solid-liquid separation is performed on the blended solid-liquid mixture crystals through gravity concentration, and different operations are carried out according to different contents of the separated crystallized materials; and 2) solid-liquid mixture crystals generated through temperature reduction or not are blended by using clear water or a circulating mother liquor by a volume ratio of 10%-80% and the liquid can be recycled, solid-liquid separation is performed on the blended solid-liquid mixture crystals through gravity concentration equipment, and different operations are carried out according to different contents of the separated crystallized materials. As a result, the quantity of potassium nitrate carried in ammonium chloride is reduced, the dosage of the clear water in the whole process is reduced, the dosage of a fuel is reduced, and considerable economic benefit can be achieved.

Description

technical field [0001] The invention relates to a production method of potassium nitrate, in particular to an improvement of a part of the production method of potassium nitrate. Background technique [0002] Now the process of producing potassium nitrate with potassium chloride and ammonium nitrate is: [0003] 1. According to the content of each substance in the circulating mother liquor or clear water, add a certain amount of potassium chloride (a certain amount of ammonium nitrate should be added when using clear water), let the above substances mix and react (heating or not). [0004] 2. For step 1: [0005] a. For the heating reaction, the solution should be cleared or cleared with a filter, and the clear solution should flow into or be pumped into the crystallizer to crystallize (the crystallization is: crystallization of mixtures such as potassium nitrate and ammonium chloride); [0006] b. For the reaction without heating, proceed directly to the next step. [00...

Claims

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Application Information

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IPC IPC(8): C01D9/10
Inventor 朱建江
Owner 朱建江
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