Recombinant human lysozyme with broad-spectrum tumor cell killing activity and its application
A human lysozyme, tumor cell technology, applied in the field of medicine, can solve the problems of non-uniformity, other characteristic differences, and anti-tumor research on the direct killing effect of human lysozyme on tumor cells has not been found.
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Embodiment 1
[0169] Human lysozyme (abbreviated as ghLZ) produced by transgenic sheep and its purification
[0170] Human lysozyme transgenic goat milk (the preparation process is the same as CN200510110772.1) 400mL, refrigerated and centrifuged at 4°C, 8000-10000rpm, centrifuged for 15-30min to defat. Remove the precipitated impurities and the fat in the upper layer, get the middle layer liquid and filter it with skimmed milk gauze to obtain the skimmed whey (SDS-PAGE analysis such as figure 1 Shown in lane 2) 300mL. An equal volume of 20 mM pH7.4 PB buffer was added thereto, the pH was adjusted to 4.6, and the mixture was bathed in water at 40° C. for 30 min. Refrigerate and centrifuge at 4°C, 8000-10000rpm, and centrifuge for 15-30min to remove casein. Collect the whey (SDS-PAGE analysis such as figure 1 Shown in swimming lane 3), the pH was adjusted to 7.4 with NaOH, and the precipitate was removed by centrifugation again, and collected after gauze filtration.
[0171] SP column (c...
Embodiment 2
[0174] Inhibitory effect of ghLZ on human gastric cancer MGC-803 cells in vitro
[0175] Adjust the density of human gastric cancer MGC-803 cells to 1×10 4 / mL, add 100 μL to 96-well culture plate, that is, 1000 cells / well. Dilute the ghLZ lyophilized powder with RPMI 1640 culture medium to a final concentration of 8 mg / mL, and filter to sterilize with a 0.22 μm filter membrane. Dilute 4-fold with RPMI 1640 culture medium to 4 mg / mL, 1 mg / mL, 0.25 mg / mL, 0.0625 mg / mL and 0.016 mg / mL, 50 μL / well. Each concentration was performed in triplicate.
[0176] At the same time, cisplatin (1mg / mL) was used as a positive control, the RPMI 1640 group without ghLZ was used as a negative control, the culture medium (no cells) and the drug group (no cells) were used as blank controls, and water was added to the surrounding wells of the 96-well culture plate to reduce The liquid in the edge hole evaporates. 37°C, 5% CO 2 Cultivate, pay attention to observation during the period. After 7...
Embodiment 3
[0179] Inhibitory effect of ghLZ on human gastric cancer BGC-823 cells in vitro
[0180] The method is the same as in Example 2, except that the cells are human gastric cancer BGC-823 cells.
[0181] The result is as Figure 4 As shown, the inhibition rate was 50.24% at 1 mg / mL, and it was determined to be active if it was greater than 50%.
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