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Preparation of graphene oxide and post-processing method for waste liquor

A graphene and graphene technology, which is applied in the fields of graphene oxide preparation and waste liquid post-treatment, can solve the problems of doubling sulfuric acid and potassium permanganate, and achieve the effects of avoiding emissions, fast preparation methods, and simplified waste liquid treatment

Inactive Publication Date: 2013-11-06
QINGDAO ZHONG KE HAO TAI NEW MATERIAL SCI & TECH
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AI Technical Summary

Benefits of technology

This patented describes methods for producing high quality single layer or multi-ayered carbon materials with specific properties such as electrical conductivity, optical transparency, hydrophilicity, chemical stability, etc., without generating harmful emissions during production processes. These techniques can be applied to various industries including electronics manufacturing, energy storage devices, environmental remediation, biomedical applications, sensors, catalyst carriers, coatings, membranes, batteries, fuel cells, wires, cables, medical implants, smart windows, electronic displays, solar panels, battery electrodes, advanced composite material technology, and other fields where precise control over these qualities has become crucial due to their potential impact on human health issues like respiratory diseases caused by indoor air contamination.

Problems solved by technology

Technological Problem: Current Method Chemistry Previous Art describes various ways to make small amounts of graphane oxide, such as making them easier to handle on larger scales. Existing techniques involve either expensive reagents or complicated procedures involving several stages.

Method used

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  • Preparation of graphene oxide and post-processing method for waste liquor
  • Preparation of graphene oxide and post-processing method for waste liquor
  • Preparation of graphene oxide and post-processing method for waste liquor

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Embodiment Construction

[0026] The present invention will be further described below in conjunction with specific examples, but the protection scope of the present invention is not limited to the following examples. The methods are conventional methods unless otherwise specified. The raw materials can be obtained from public commercial sources unless otherwise specified.

[0027] The preparation method of the present invention improves the Hummers method without adding sodium nitrate at all. The specific implementation steps are: mix 3.0 g of natural graphite powder (325 mesh) with 70 mL of 98wt% concentrated sulfuric acid in an ice-water bath, and slowly add 9.0 g of potassium permanganate after stirring evenly. The entire adding speed is controlled at about 20 minutes, and then Stirring was continued for 10 minutes, and the reaction mixture was stirred and reacted at 40° C. for 30 minutes. 140 mL of deionized water was added to the reaction solution, and after the temperature was raised to 95° C....

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Abstract

The invention relates to a preparation method for graphene oxide. The preparation method comprises the following steps: a. mixing a graphite powder and concentrated sulfuric acid at the low temperature; b. adding potassium permanganate, and heating to carry out an intermediate temperate reaction; c. adding water for a high temperature reaction, d. adding hydrogen peroxide aqueous solution for a reaction, and after finishing the reaction, filtering the obtained bright yellow solution; e. washing the filter cake with HCl aqueous solution; f. after drying the obtained solid, putting into water for stirring, and dialyzing; and g. removing a substrate by a centrifugal way to obtain a stable dispersion liquid of graphene oxide.

Description

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Claims

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Application Information

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Owner QINGDAO ZHONG KE HAO TAI NEW MATERIAL SCI & TECH
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