Pineapple fiber pulp and preparation method thereof

A technology of pineapple hemp and pulp, which is applied in the direction of pulp beating method, pulping with inorganic alkali, non-woody plant/crop pulp, etc. It can solve the problem that it is difficult to ensure the uniformity of fibers, and the properties of pineapple hemp fibers are not the same, and cannot Adopt complete degumming method and other problems to achieve the effect of improving commercial utilization value, shortening production cycle, avoiding difficult circulation and continuous foaming problems

Active Publication Date: 2014-01-08
潍坊欣龙生物材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] (1) The single fiber length of pineapple hemp fiber is very short, the single fiber length is 3-8mm, and the complete degumming method cannot be used, and the semi-degumming method must be used to ensure that there is a certain amount of residual glue, and the very short single fiber is bonded to meet the requirements of spinning. The long fibers required by the yarn process, so the uniformity of the fibers will be difficult to guarantee
[0004] (2) Using chemical degumming method, serious environmental pollution, low product quality level, high production cost
[0006] (4) Due to different varieties and different origins, the properties of pineapple hemp fibers are different, which has a great impact on processing
[0007] Due to the existence of the above problems, the application of pineapple fiber in some fields such as clothing, especially underwear, is limited. Therefore, the commercial value of the development and application of pineapple is not high at present.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] (1) Pretreatment: Cut the pineapple hemp into 3-5cm long pieces, and then wash and remove impurities.

[0033] (2) Cooking: After the pretreated pineapple hemp is pretreated by a combing machine, it is put into the digester, and sodium hydroxide of 8% relative to the absolute dry pineapple hemp weight and 8% relative absolute dry pineapple hemp weight are added. Hydrogen peroxide, 0.2% of magnesium sulfate relative to the absolute dry weight of pineapple hemp, and 1.5% of sodium silicate relative to the absolute dry weight of pineapple hemp, the liquid ratio is 1:3.5, and the cooking time is 160min.

[0034] (3) Washing: Wash the cooked pineapple and hemp pulp in a vacuum washer. The feeding concentration of the pineapple and hemp pulp is 2.0 wt %, and the drum rotation speed of the vacuum washer is 1.5 r / min, the washing temperature was 65°C, the washing time was 30 min, and the pulp concentration after washing was 9 wt%.

[0035] (4) Beating: The washed pineapple an...

Embodiment 2

[0040] (1) Pretreatment: Cut the pineapple hemp into 3-5cm long pieces, and then wash and remove impurities.

[0041](2) Cooking: put the pretreated pineapple hemp into the digester after being pretreated by a combing machine, add 10% sodium hydroxide relative to the absolute dry pineapple hemp weight, and 10% relative absolute dry pineapple hemp weight. Hydrogen peroxide, 0.4% of magnesium sulfate relative to the absolute dry weight of pineapple hemp, and 2.5% of sodium silicate relative to the absolute dry weight of pineapple hemp, the liquid ratio is 1:4, and the cooking time is 220min.

[0042] (3) Washing: Wash the cooked pineapple and hemp pulp in a vacuum washer. The feeding concentration of the pineapple and hemp pulp is 1.8 wt%, and the drum rotation speed of the vacuum washer is 1.8 r / min, the washing temperature was 68 °C, the washing time was 35 min, and the slurry concentration after washing was 11 wt%.

[0043] (4) Beating: The washed pineapple and hemp pulp is...

Embodiment 3

[0048] (1) Pretreatment: Cut the pineapple hemp into 3-5cm long pieces, then wash and remove impurities. The sulfuric acid insoluble matter in the pineapple hemp after removal of impurities is 8.0wt%, the ash content is 2.3%, and the iron content is 620mg / kg.

[0049] (2) Cooking: After the pretreated pineapple hemp is pretreated by a combing machine, it is put into the digester, and 5% sodium hydroxide relative to the absolute dry pineapple hemp weight and 4% relative absolute dry pineapple hemp weight are added. Hydrogen peroxide, 0.01% magnesium sulfate relative to the weight of absolutely dry pineapple hemp, and 1% sodium silicate relative to the weight of absolutely dry pineapple hemp, the liquid ratio is 1:3, and the cooking is carried out. Steam was introduced into the vessel for cooking, the cooking heating time was 30 minutes, the temperature was 100°C, and the holding time was 40 minutes. During the heat preservation process, the steam is released once to remove the ...

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PUM

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Abstract

The invention discloses pineapple fiber pulp and a preparation method thereof. Pineapple fibers are taken as raw materials of the pineapple fiber pulp. The preparation method comprises the following steps: preprocessing, integrating stewing and bleaching, washing by a vacuum washer continuously beating, carrying out pressure sieving twice, carrying out acid treatment, washing by water, and pulping to obtain the pineapple fiber pulp. According to the preparation method, the pineapple fiber pulp is prepared from the pineapple fibers; the stewing and bleaching processes are integrated, so that the operation is simple and convenient, the production cycle is remarkably shortened while the stewing and bleaching quality is guaranteed, the production process is simple, the flow process is short, the energy consumption is low, indexes such as CODcr (chemical oxygen demand) in a stewed black solution are remarkably lowered in comparison with those in a conventional process, and the wastewater treatment cost is reduced; prepared regenerated cellulose viscose fibers have excellent performance of general viscose fibers, fabrics of the regenerated cellulose viscose fibers remain the bacterial resisting and inhibiting performance of raw hemp, and thus the commercial exploitation value of the pineapple fibers is improved.

Description

technical field [0001] The invention relates to pulp for regenerated cellulose fibers, in particular to a pulp used for producing regenerated cellulose fibers by using pineapple hemp as a raw material. Background technique [0002] Pineapple is widely planted in tropical countries and regions, and people mainly use its fruit. A large number of pineapple hemp leaves become agricultural waste and are burned, which not only causes waste of resources, but also causes environmental pollution. With the rapid increase in the demand for natural fibers in the world market, the waste of pineapple and hemp resources has received extensive attention. Many countries, such as Japan, the United States, India, the Philippines and Taiwan, have begun to develop and utilize pineapple and hemp fibers and have achieved some commercial As a result, my country also started research on the extraction and application of pineapple hemp fiber in the late 1990s. After degumming, medium and low-grade ble...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D21H11/12D21C3/02D21C9/02D21D1/02D21D5/02
Inventor 秦翠梅王乐军马君志李昌垒姜明亮王东徐海鹏
Owner 潍坊欣龙生物材料有限公司
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