Synthetic method of weak acidic red dye
A technology of red dye and synthesis method, which is applied in the field of weak acid red dye synthesis, can solve the problems of poor color fastness and large migration of dyed leather, achieve good color fastness, light chroma, and reduce processing costs Effect
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[0012] Example 1:
[0013] A method for synthesizing weak acid red dye, using the following steps:
[0014] 1) Diazotization: After mixing p-aminoazobenzene hydrochloride, hydrochloric acid and sodium nitrite, the reaction time is 20 minutes at a temperature of 40°C and 2≤PH≤4;
[0015] 2) Coupling: add soda ash after diazotization of p-aminoazobenzene hydrochloride, hydrochloric acid and sodium nitrite, react for 2 hours under the conditions of 20℃, 8≤PH≤10, add the diazotized diazonium The diazonium salt of aminobenzenesulfonanilide, react for 2 hours at a temperature of 30℃, 8≤PH≤10, add sodium sulfate after the second coupling, at a temperature of 20℃, 8≤PH≤10 , Reaction for 2 hours;
[0016] 3) Filtration: remove the filter residue;
[0017] 4) Drying: drying after filtering to produce finished products.
[0018] The mass ratio of the aminoazobenzene hydrochloride, hydrochloric acid, sodium nitrite to the soda ash and sodium sulfate is 2:3:2:3:5. Example one
Example Embodiment
[0012] Example 1:
Example Embodiment
[0019] Example 2:
[0020] A method for synthesizing weak acid red dye, using the following steps:
[0021] 1) Diazotization: After mixing p-aminoazobenzene hydrochloride, hydrochloric acid and sodium nitrite, the reaction time is 30 minutes at a temperature of 45°C and 2≤PH≤4;
[0022] 2) Coupling: add soda ash after diazotization of p-aminoazobenzene hydrochloride, hydrochloric acid, and sodium nitrite, react for 3 hours at a temperature of 25°C, 8≤PH≤10, and add the diazotized diazonium Diazonium salt of aminobenzenesulfonanilide, react for 3 hours at a temperature of 40℃, 8≤PH≤10, add sodium sulfate after the second coupling, at a temperature of 40℃, 8≤PH≤10 , React for 3 hours;
[0023] 3) Filtration: remove the filter residue;
[0024] 4) Drying: drying after filtering to produce finished products.
[0025] The mass ratio of the aminoazobenzene hydrochloride, hydrochloric acid, sodium nitrite to the soda ash and sodium sulfate is 2:3:2:3:5.
[0026] The advantages of the invention...
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