Assay for the detection of nucleotide substitutions in the genome of the Sabin oral poliovirus vaccine virus
A polio and genome technology, applied in the field of kits containing the above primers, can solve the problems of expensive, non-existent fast and convenient tests, etc.
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Embodiment 1
[0116] Preparation of DNA amplicons from three serotypes of poliovirus
[0117] Poliovirus of each serotype (type 1, 2 or 3) was obtained separately. Poliovirus samples, cDNA, were synthesized from frozen infected cultures using antisense PCR primers and DNA amplicon generation in a single multiplex reverse transcription and PCR reaction (Roche). PCR products (DNA amplicons) were purified by PCR purification kit (Quagcn).
[0118] RT-PCR - For RT-PCR analysis, direct frozen infection cultures (1fll) and 67mM Tris / HCl (pH 8.8), 17mM Ammonium Sulfate, 6mM EDTA, 2mM MgCh, 200Mm each dNTP, 1mM dioxane in a total volume of 50fll were taken directly. Thiothreitol, 1 mM of each primer, 10 U placental RNase inhibitor (Roche), 3 U avian myeloblastosis virus (AMV) reverse transcriptase (Roche), and 5 U Taq DNA polymerase (Roche AppliedScience). Reactions were incubated at 50°C for 30 minutes, followed by 3 minutes at 94°C. 35 thermal cycles of 94 °C for 30 s, 42 °C for 30 s, 72 °C fo...
Embodiment 2
[0120] Single Nucleotide Polymorphism Assay (SNP Assay) for Mutation Identification
[0121]Ten SNP reactions were performed in a final volume of 10III containing SNaPshot multiplex ready-to-use reaction mix (5lll), primer mix (3lll) (final concentration, 0.15-0.6Ilmolll) and template (2llll) prepared by QIAquickPCR as described above. Purification kit (Qiagcn) purified multiplex PCR product composition. Multiplex PCR products amplified from viral RNA were pooled and purified on the same column prior to the SNaPshot reaction. The cycling program consisted of 25 cycles of 96 °C for 10 s, 50 °C for 5 s and 60 °C for 30 s. Extension products were purified by inactivating the enzyme by incubating with 1 U shrimp alkaline phosphatase for IS-min at 37°C, followed by incubation for IS-min at 75°C. The purified product (0.5111) was mixed with 9III formamide and 0.5III GeneScan-120LIZ size standard (Applied Biosystems) and separated by capillary electrophoresis (ABIPRISM3130 GeneticA...
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