A kind of bile acid composition and preparation method thereof
A bile acid and composition technology, applied in the field of bile acid composition and its preparation, can solve the problems of farmers' economic loss, large consumption of reagents, difficult industrialization, etc. mild effect
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Embodiment 1
[0021] The bile acid composition, its active ingredient composition comprises hyodeoxycholic acid, hyodeoxycholic acid and chenodeoxycholic acid, the weight percent of the sum of hyodeoxycholic acid and hyodeoxycholic acid is 80.0%, and chenodeoxycholic acid The percentage by weight of the weight percentage is 18.0%, and the rest is moisture and ash (the sum of the percentage by weight is calculated as 100%).
[0022] The preparation method of this bile acid composition adopts the following steps:
[0023] (1) Saponification: Add 500 kg of pig gall powder crushed through a 40-mesh sieve into the reactor, then add 5000 L of sodium hydroxide solution with a mass fraction of 10%, heat and stir, and start when the solution in the reactor is heated to 100°C Timing, continue heating and stirring to keep the boiling state for 12 hours, then cool the saponified liquid generated by the reaction until the solid-liquid layer is separated, and use a pipeline centrifugal pump to centrifuga...
Embodiment 2
[0030] The bile acid composition, its active ingredient composition comprises hyodeoxycholic acid, hyodeoxycholic acid and chenodeoxycholic acid, the weight percentage of the sum of hyodeoxycholic acid and hyodeoxycholic acid is 78.0%, and chenodeoxycholic acid The percentage by weight of the weight percentage is 20.0%, and the rest is moisture and ash (the sum of the percentage by weight is calculated as 100%).
[0031] The preparation method and consumption are the same as in Example 1.
Embodiment 3
[0033] The bile acid composition, its active ingredient composition comprises hyodeoxycholic acid, hyodeoxycholic acid and chenodeoxycholic acid, the weight percent of the sum of hyodeoxycholic acid and hyodeoxycholic acid is 79.0%, and chenodeoxycholic acid The percentage by weight of the weight percentage is 20.0%, and the rest is moisture and ash (the sum of the percentage by weight is calculated as 100%).
[0034] The preparation method and consumption are the same as in Example 1.
[0035] During the preparation of the bile acid composition, crude bile acid composition is obtained through crude extraction. In the crude product, there are many kinds of bile acid compositions and are complex. In order to make the effect of the bile acid composition in livestock and poultry more obvious, through two steps of purification and recrystallization, other bile acids in the crude product of the bile acid composition , such as lithocholic acid, deoxycholic acid, etc., are removed f...
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