Refrigerator and method of manufacturing the same
A technology for refrigerators and space parts, applied in the field of refrigerators and their manufacturing, can solve problems such as complex structures and manufacturing processes
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preparation example 1
[0105] [Preparation Example 1] Preparation of reactive opening composition
[0106] In a 3L reaction vessel, add the formulation for preparing polyurethane foam, 700g of silicone oil used as a surfactant, and 277.9g of 12-hydroxystearic acid (12HSA), and heat the resulting solution to about 100°C while stirring at 1880rpm to 3600rpm . Subsequently, a solution of 22.1 g of lithium hydroxide (LiOH) dissolved in 100 ml of distilled water at 70° C. was slowly added over a period of 30 minutes to induce an acid-base neutralization reaction. After the reaction was completed, the temperature of the reaction vessel was gradually raised to 200° C., and the reaction product was stirred for 1 hour to completely remove moisture contained in the reaction product. Then, the reaction product was slowly cooled to about 60° C. and post-treated using a roller mill and a filter to prepare a combination having a solid content of 30% by weight and including a combination of a grease-type surfacta...
experiment example 1 and experiment example 2 and comparative example 1
[0109][Experimental Example 1 and Experimental Example 2 and Comparative Example 1] Preparation of Rigid Polyurethane Foam
[0110] According to the quantities quantified by the composition ratios shown in Table 2, the ingredients shown in Table 2 below were mixed at room temperature (25° C.) using a mechanical mixer at high speed for 4 to 5 seconds, and the resulting mixture was poured into An open mold with a size of 20 x 20 cm and a rectangular shape was used to induce foam formation. After the reaction was completed, the formed foam was aged for 24 hours and cut, and the cell size was measured with a scanning electron microscope (SEM), and is shown in Table 2.
[0111] In addition, Table 3 below shows measurement results of properties of polyurethane foams prepared according to Experimental Example 1 and Experimental Example 2 and Comparative Example 1.
[0112] [Table 2]
[0113]
[0114]
[0115] [table 3]
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[0117] As shown in Table 3, it could be co...
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