A kind of preparation method of activated carbon shaped filter element with bactericidal function
The technology of activated carbon and filter element is applied in the field of preparation of activated carbon filter element.
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Embodiment 1
[0019] 1. Put the activated carbon filter element into the mixed solution of 0.2% sulfuric acid and 0.3% hydrogen peroxide for immersion cleaning or pressure flushing for 10-20 minutes, take it out, and after centrifugal dehydration, place it in a vacuum drying oven at 80-100°C for later use.
[0020] 2. Put the molded filter element that has been dried and removed the surface reductivity into a silver nitrate solution with a concentration of 0.1% and let it stand for 30 minutes to allow it to fully absorb, then centrifugally dehydrate it, and dry it in a vacuum drying oven at 80-85°C for 4 Stand by after hours.
[0021] 3. Weigh 25 grams each of potassium persulfate and sodium hydroxide, dissolve them in 500 milliliters of pure water, and heat to 80°C as the reaction solution.
[0022] 4. Take out the activated carbon filter element impregnated and adsorbed silver from the drying oven, place it in the heated reaction liquid for 30-40 minutes of chemical reaction, take it out ...
Embodiment 2
[0025] 1. Remove the surface reducibility of the filter element according to Step 1 of Example 1.
[0026] 2. Put the filter element in step 1 into 0.3% silver nitrate solution for immersion, let it stand for full absorption, and then dehydrate and dry for 6 hours.
[0027] 3. Weigh 24 grams each of potassium persulfate and sodium hydroxide, dissolve them in 500 milliliters of pure water, and heat to 85°C to make the reaction solution.
[0028] 4. Put the filter elements treated in steps 1 and 2 in the reaction liquid, react in the reaction liquid at 85°C for 40 minutes, and keep warm for 45 minutes.
[0029] 5. Take out the filter element from the reaction solution and wash it with pure water (remove the by-products sodium sulfate, potassium sulfate and potassium nitrate (sodium) produced by the reaction) until the pH value of the washing solution is 7.5, dehydrate and dry to constant weight to obtain the finished product.
Embodiment 3
[0031] 1. Remove the surface reducibility of the filter element according to Step 1 of Example 1.
[0032] 2. Place the dried filter element in step 1 in a silver nitrate solution with a concentration of 0.5% and let it stand for 30 minutes to fully absorb, then dehydrate and dry for 5 hours.
[0033] 3. Weigh 48 grams each of potassium persulfate and sodium hydroxide, dissolve them in 1000 milliliters of pure water, and heat to 90°C as the reaction solution.
[0034] 4. Place the filter element treated in steps 1 and 2 in the reaction solution at 90°C for 30 minutes and keep it warm for 40 minutes.
[0035] 5. Take out the filter element from the reaction solution and rinse it with pure water until the pH value of the rinse solution is 8.5, dehydrate and vacuum dry at 105°C to obtain the product.
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