Adhesive for PVC (Polyvinyl Chloride) pipes and preparation method thereof
An adhesive and effective technology, applied in the direction of adhesives, adhesive additives, non-polymer adhesive additives, etc., can solve the problems of energy consumption, complicated welding process, long curing time, etc.
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[0018] The present invention also provides a preparation method of an adhesive for PVC pipes, the preparation method comprising:
[0019] a, soaking perchlorethylene resin and polyvinyl chloride resin in a mixed solution comprising butyl acetate, cyclohexanone and ethylene dichloride to prepare a basic mixed solution;
[0020] b. Mix and soak the alkyd resin, dibutyl phthalate and the basic mixed liquid to prepare the modified mixed liquid;
[0021] c. Add light calcium carbonate to the modified mixture to form an adhesive for PVC pipes.
[0022] In the preparation method of the PVC pipe adhesive provided by the present invention, the amount of each raw material can be selected in a wide range, but in order to make the PVC pipe adhesive have more excellent viscosity, bonding strength and hydraulic burst strength . Preferably, relative to 100 parts by weight of perchlorethylene resin, the amount of polyvinyl chloride resin is 30-80 parts by weight, the amount of butyl acetate...
Embodiment 1
[0031] a. At 25°C, soak 100 parts by weight of perchlorethylene resin and 50 parts by weight of polyvinyl chloride resin in a mixed solution containing 300 parts by weight of butyl acetate, 500 parts by weight of cyclohexanone and 200 parts by weight of ethylene dichloride 2.5h to prepare the basic mixed solution; wherein, the weight average molecular weight of the perchlorethylene resin is 3000-5000, and the weight average molecular weight of the polyvinyl chloride resin is 7500.
[0032] b. At 25°C, mix 50 parts by weight of alkyd resin and 20 parts by weight of dibutyl phthalate with the above basic mixed solution and soak for 2.5 hours to obtain a modified mixed solution; the weight average of alkyd resin The molecular weight is 8000, and the particle size of light calcium carbonate is 0.02mm.
[0033] c. Add 1500 parts by weight of light calcium carbonate to the above-mentioned modified mixed solution to form PVC pipe adhesive A1.
[0034] The parameters of the viscosity...
Embodiment 2
[0036] a. At 20°C, soak 100 parts by weight of perchlorethylene resin and 30 parts by weight of polyvinyl chloride resin in a mixed solution containing 250 parts by weight of butyl acetate, 300 parts by weight of cyclohexanone and 150 parts by weight of ethylene dichloride 2h to prepare the basic mixed liquid; wherein, the weight average molecular weight of the perchlorethylene resin is 3000, and the weight average molecular weight of the polyvinyl chloride resin is 7000.
[0037] b. At 20°C, mix 30 parts by weight of alkyd resin and 10 parts by weight of dibutyl phthalate with the above basic mixed solution and soak for 2 hours to obtain a modified mixed solution; the weight average molecular weight of alkyd resin 4000, the particle size of light calcium carbonate is 0.01mm.
[0038] c. Add 1400 parts by weight of light calcium carbonate to the above-mentioned modified mixed solution to form PVC pipe adhesive A2.
[0039] The parameters of the viscosity, bond strength and hy...
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