Fixation method for Chinese medicinal herbs or tea leaves
A technology of greening and medicinal materials, which is applied in the direction of making drugs into special physical or ingestible devices, tea treatment before extraction, etc., can solve the problem of low chlorogenic acid content, and achieve simple processing methods, nutritional value and medicinal value. Effects with high value and good application prospects
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preparation example Construction
[0026] Preparation of the reference solution. Accurately weigh an appropriate amount of chlorogenic acid, place it in a brown measuring flask, and add 50% methanol to make a solution containing 40μg per 1ml.
[0027] Preparation of the test solution: pulverize the dried honeysuckle, pass through a No. 4 sieve, take about 0.5g of the powder, accurately weigh it, and place it in a conical flask with a stopper. Add 50% methanol 50ml accurately, weigh it, and ultrasonic treatment (power 250W, frequency 35kHz) for 30 minutes, let it cool, then weigh it, use 50% methanol to make up the lost weight, shake, filter, accurately measure 5ml of the filtrate, place it in a 25ml brown measuring flask, and add 50% methanol To the mark, shake well, ready to go.
[0028] The determination method accurately draws 10ul of the reference solution and the test solution respectively, and injects them into the liquid chromatograph for detection.
Embodiment 1
[0029] Example 1 The method for curing of the present invention
[0030] (1) The fresh tea leaves, remove the sundries, and seal them in a plastic bag;
[0031] (2) Put the sealed fresh tea leaves in an ultra-high pressure container for ultra-high pressure treatment, the pressure is 300 MPa, and the time is 20 minutes.
Embodiment 2
[0032] Example 2 The method for curing of the present invention
[0033] (1) Remove the sundries from the fresh honeysuckle after picking, and seal it in a flexible plastic bucket;
[0034] (2) Put the sealed fresh honeysuckle in an ultra-high pressure container for ultra-high pressure treatment, the pressure is 100 MPa, and the time is 30 minutes.
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