Epoxy resin adhesive and flexible copper clad laminate prepared by the adhesive and preparation method
A technology of flexible copper clad laminate and epoxy resin, applied in the direction of online phenolic epoxy resin adhesive, adhesive type, aldehyde/ketone condensation polymer adhesive, etc., can solve the problem of poor heat resistance and difficulty in ensuring metallization Hole thermal shock resistance, limited use range, etc.
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Embodiment 1
[0013] formula parts by mass Multifunctional epoxy resin 100 Nitrogen-containing phenolic resin curing agent 100 High dielectric constant filler 40 A silane coupling agent 1 Defoamer 1
[0014] According to the preparation process of the present invention and the above ratio, after mixing 100 parts of multifunctional epoxy resin with 40 parts of high dielectric constant filler, 1 part of silane coupling agent and 1 part of defoamer at 80 ° C, add 100 parts of nitrogen phenolic resin curing agent, co-heated to make a uniform liquid, degassed, poured into a mold, kept at 120 ° C for 2 hours, raised to 150 ° C and kept for 4 hours, and then released from the mold to cool, and the resin sample was obtained; Get FCCL samples.
Embodiment 2
[0016] formula parts by mass Multifunctional epoxy resin 100 Nitrogen-containing phenolic resin curing agent 80 High dielectric constant filler 40 A silane coupling agent 1 Defoamer 0.7
[0017] In parts by weight, after mixing 100 parts of the prepared multifunctional epoxy resin with 40 parts of high dielectric constant filler, 1 part of silane coupling agent and 0.7 part of defoamer at 60 ° C, add nitrogen-containing phenolic resin 80 parts of curing agent were heated together to make a uniform liquid, degassed, poured into a mold, kept at 110°C for 2 hours, raised to 160°C and kept for 4 hours, and then released from the mold to cool to obtain a resin sample; and FCCL samples were obtained .
Embodiment 3
[0019] formula parts by mass Multifunctional epoxy resin 100 Nitrogen-containing phenolic resin curing agent 70 High dielectric constant filler 40 A silane coupling agent 0.8 Defoamer 1
[0020] In parts by weight, mix 100 parts of the prepared multifunctional epoxy resin with 40 parts of high dielectric constant fillers, 0.8 parts of silane coupling agent, and 1 part of defoamer at 70 ° C, and then add nitrogen-containing phenolic resin 70 parts of curing agent were heated together to make a uniform liquid, degassed, poured into a mold, kept at 115°C for 2 hours, raised to 150°C and kept for 4 hours, then released from the mold and cooled to obtain a resin sample; and FCCL samples were obtained .
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