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Improved DMTO reactor

A reactor and improved technology, which is applied in the field of improved DMTO reactors, can solve the problems of increasing secondary reactions of olefins, bed fluctuations, back-mixing, etc., and achieve the reduction of catalyst concentration, reduction of secondary reactions, and reduction of catalyst amount Effect

Inactive Publication Date: 2015-08-05
宁波富德能源有限公司
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  • Abstract
  • Description
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AI Technical Summary

Problems solved by technology

Such a catalyst distribution is not suitable for the DMTO reaction, too much catalyst is distributed from the transition section to the top of the dilute bed, serious back-mixing, and secondary conversion of olefins are easy to occur, all of which affect the olefin selectivity of methanol
The reason for the above problems is that the DMTO reactor works in the bubbling bed state, the bubbles cause a large amount of entrainment, the bubbles break at the bed interface, and part of the catalyst is ejected into the dilute phase, thereby increasing the density of the catalyst in the dilute phase , increasing the secondary reaction of alkenes
At the same time, the rupture of large bubbles will cause a large disturbance to the air flow, resulting in large fluctuations in the bed and serious back mixing.
All of the above will affect the selectivity of methanol to olefins, thereby reducing the yield of olefins

Method used

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Embodiment approach

[0013] Figure II Shown is a second embodiment of the invention. The difference from the first embodiment is that in this embodiment, the two layers of grids are arranged on the upper part of the dense bed, and their heights are lower than the bed interface. This setting avoids interference with the heat collector in the dense-phase bed, and at the same time effectively reduces the size of the air bubbles reaching the bed interface, so that there is less catalyst entrained, reducing the pressure in the dilute-phase bed. The catalyst concentration is low, reducing the occurrence of secondary reactions; reducing the disturbance of the bed interface caused by bubble breakage, improving the stability of the bed and reducing the occurrence of back mixing. Through the above optimization, the yield of olefins is improved.

[0014] Compared with the prior art, the present invention has the following beneficial effects: the present invention arranges grids in the dense-phase bed area...

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Abstract

The invention discloses an improved DMTO reactor. According to the invention, by means of arrangement of a grating in a dense-phase bed layer zone of the DMTO reactor, entrainment amount of a catalyst is reduced and the concentration of the catalyst in a dilute-phase bed layer is reduced, so that a secondary reaction is reduced. Meanwhile, bubbles are reduced in size so that the disturbance on the bed layers is reduced when the bubbles are broken, so that the bed layers are more stable and reduced in backmixing. By means of the technical scheme, selectivity of methanol to olefin is increased, thereby increasing the yield of olefin.

Description

technical field [0001] The invention relates to the field of chemical equipment, in particular to an improved DMTO reactor. Background technique [0002] DMTO is a method of producing low-carbon olefins through methanol under the action of a catalyst. The reaction occurs on the surface of the catalyst, and a large amount of heat is released during the reaction. At the same time, the coke produced by the reaction is accumulated on the surface of the catalyst, so that the catalyst is quickly deactivated, and the catalyst can recover its activity after being burnt. The gas and solid phase fluidized bed catalytic reactor has the advantages of high catalytic conversion rate, uniform temperature distribution in the bed, and convenient catalyst replacement. These advantages are just in line with the DMTO process, and the natural gas and solid phase fluidized bed catalytic reactor has become the preferred reactor for the DMTO process. The distribution of the catalyst inside the ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J8/24
Inventor 季兆臣魏晓峰张武军张建光周平
Owner 宁波富德能源有限公司
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