Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Diamond anvil cell pressing machine trace gas liquefying plant

A technology of diamond-topping and trace gas, which is applied in the field of gas liquefaction equipment, can solve the problems of unsafety and consumption of a large amount of gas, and achieve the effect of improving the environment and eliminating hidden dangers of unsafety

Inactive Publication Date: 2015-08-05
JILIN UNIV
View PDF5 Cites 5 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The technical problem to be solved by the present invention is to overcome the shortcomings of the prior art that consume a large amount of gas and be unsafe. In the diamond counter-anvil (DAC) press, the technology of micro gas liquefaction is adopted to design a diamond counter-anvil press with a small amount of gas. Gas liquefaction device, realizing the packaging of flammable, explosive and expensive gas samples in the DAC press

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Diamond anvil cell pressing machine trace gas liquefying plant
  • Diamond anvil cell pressing machine trace gas liquefying plant
  • Diamond anvil cell pressing machine trace gas liquefying plant

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] figure 2 A schematic cross-sectional view of the low temperature chamber 4 of the present invention is given. The cryogenic chamber can be in the shape of a cylinder, and the upper bottom surface is open for putting into the DAC press, and the upper end can be processed with protruding edges to prevent it from falling into the liquid nitrogen chamber 8 when it is put into the round hole in the middle of the upper cover 2 . The low temperature chamber 4 matches the overall appearance size and shape of the DAC compressor, so that the DAC compressor loaded therein can be cooled by liquid nitrogen faster. There is a gas inlet 5 on the edge protruding outwards, that is, the gas enters the passage of the diamond anvil sample cavity, the inner port of the gas inlet 5 can be docked with the observation hole on the side of the press, and the outer port of the gas inlet 5 can be connected with Gas cylinder 14 communicates.

[0024] image 3 A schematic cross-sectional view o...

Embodiment 2

[0027] Figure 5 The structure in which the liquid nitrogen circulation system and the low-temperature chamber of the diamond anvil press trace gas liquefaction device of the present invention are assembled together is given. Figure 5 Among them, 1 is the cavity jacket, 2 is the upper cover, 3 is the liquid nitrogen inlet, 4 is the cryogenic chamber, 5 is the gas inlet, 6 is the liquid nitrogen outlet, 7 is the cryogenic sealing ring, and 8 is the liquid nitrogen chamber.

[0028] Among them, the three parts outside the chamber 1, the upper cover 2 and the low temperature chamber 4 need to be tightly matched. The liquid nitrogen inlet 3 and the liquid nitrogen outlet 6 can be welded integrally with the upper cover by adopting stainless steel ferrule joints. A low-temperature sealing ring 7 can be installed between the cavity casing 1 and the upper cover 2, and the cavity casing 1 and the upper cover 2 are fixed and sealed by fastening bolts to prevent liquid nitrogen from se...

Embodiment 3

[0030] Figure 6 An overall structure diagram of the present invention is provided, Figure 6 Among them, 9 is a liquid nitrogen barrel, 10 is a liquid nitrogen injection pipe, 11 is a gas volume control valve, 12 is a gas injection pipe, 13 is a pressure reducing valve, 14 is a gas cylinder, 15 is a nitrogen exhaust control valve, and 16 is a nitrogen exhaust pipe .

[0031] Will Figure 5 The cavity part of the liquid nitrogen circulation system shown is connected as a whole through the liquid nitrogen barrel 9, the liquid nitrogen injection pipe 10, the nitrogen gas removal control valve 15 and the nitrogen gas removal pipe 16 to form the liquid nitrogen circulation system of the present invention. Pour liquid nitrogen into the liquid nitrogen barrel 9, and cool down the cryogenic chamber 4 and the diamond anvil press through this circulation system.

[0032] Figure 6 The gas volume control valve 11 in it, the gas injection pipe 12, the liquefied gas path formed by the...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention belongs to the technical field of gas trace liquefying encapsulation in a diamond anvil cell pressing machine and relates to a diamond anvil cell pressing machine trace gas liquefying plant. The diamond anvil cell pressing machine trace gas liquefying plant comprises a cavity outer sleeve (1), an upper cover (2) and a low-temperature chamber (4), wherein the low-temperature chamber (4) is mounted in an opening in the middle of the upper cover (2); the upper cover (2) is provided with a liquid nitrogen inlet (3) and a liquid nitrogen outlet (6); the space enclosed by the outer sleeve (1), the upper cover (2) and the low-temperature chamber (4) is a liquid nitrogen chamber (8); the diamond anvil cell pressing machine is disposed in the low-temperature chamber (4), and a gas inlet (5) is formed in the lateral side of the low-temperature chamber (4) and can be communicated with a sample chamber in the diamond anvil cell pressing machine. The diamond anvil cell pressing machine trace gas liquefying plant has the advantages that the liquid nitrogen is used to cool the low-temperature chamber (4) and the diamond anvil cell pressing machine, and when temperature reaches the liquefying temperature of encapsulation gases, the gases are injected into the sample chamber; liquefied gases are saved greatly as compared with the prior art, and potential safety hazards of inflammable and explosive gases can be eliminated.

Description

technical field [0001] The invention relates to the technical field of a gas liquefaction device, and is particularly suitable for a device for liquefying trace gas samples in a diamond counter-anvil press. Background technique [0002] As early as 1784, the British chemist Lavoisier had predicted: Suppose the earth suddenly enters a cold region, the air will undoubtedly no longer exist in the form of an invisible fluid, and it will return to a liquid state. Since then, Lavoisier's prophecy has inspired people to achieve the liquefaction of gases and thus achieve the extremely low temperature that turns gases into liquids. It sounds like a myth, but scientists not only believed it, they made it a reality. [0003] To liquefy a gas requires a sufficiently low temperature heat source. First, the sensible heat of the gas is absorbed by a low-temperature heat source, and the gas is cooled to its condensation temperature, at which point the gas becomes a saturated vapor. Then ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/42
Inventor 陆国会周强崔田黄晓丽陆冬筱
Owner JILIN UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com