Semi-dull high-intensity low-elongation viscose fiber and preparing method thereof

A viscose fiber, high-strength and low-elongation technology, which is applied in the field of semi-dull high-strength and low-elongation viscose fiber and its preparation, can solve the problem that there is no greater limit to meet the downstream new textile development and industrial upgrading, and the market share of viscose fiber decreases. and other issues, to achieve the effect of high product strength, good color fastness of finished products, and product quality improvement

Active Publication Date: 2015-08-19
YIBIN GRACE GROUP CO LTD +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] Only the above-mentioned published patent documents can know that in order to produce differentiated and functional viscose fibers, the prior art is realized by changing the production process, which involves raw materials, viscose molding and its process parameters Compared with ordinary viscose fiber, the obtained viscose fiber has been properly optimized in terms of fineness and strength, but for the increasingly fierce market competition, the differentiated viscose fiber does not meet the downstream needs to a greater extent. The development of new textiles and industrial upgrading, especially the development of fiber raw materials such as tencel, modal, and cupro fibers, which are also regenerated from natural cellulose materials, have reduced the market share of viscose fibers.

Method used

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  • Semi-dull high-intensity low-elongation viscose fiber and preparing method thereof
  • Semi-dull high-intensity low-elongation viscose fiber and preparing method thereof
  • Semi-dull high-intensity low-elongation viscose fiber and preparing method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0063] The pulp raw material is sequentially soaked, ground, crushed, kneaded, depolymerized, yellowed, dissolved, filtered, defoamed, matured, matting agent is added, spinning and drawing, refining and drying to obtain semi-dull viscose. Adhesive fiber, the semi-dull high-strength low-elongation viscose adhesive fiber of the present embodiment has the following performance index system:

[0064] The fineness is 1.67 dtex, the dry breaking strength is 3.12 cN / dtex, the wet breaking strength is 1.65cN / dtex,

[0065] The strength required to produce 5% elongation in wet state is 0.55cN / dtex,

[0066] Dry elongation at break is 19.0%, wet elongation at break is 21.0%,

[0067] The crystallinity is 40%, the radial water swelling degree is 22%, and the content of matting agent is 0.1%.

[0068] The linear density deviation rate is -11.0%, the residual sulfur is 8.0mg / 100g,

[0069] The length deviation rate is -11.0%, the ultra-long fiber rate is 0.48%, and the whiteness is 84.1...

Embodiment 2

[0072] The difference between the semi-dull high-strength low-elongation viscose fiber of the present embodiment and embodiment 1 is: the present embodiment has the following indicators:

[0073] Denier is 1.52 dtex, dry breaking strength is 3.15 cN / dtex, wet breaking strength is 1.67cN / dtex,

[0074] The strength required to produce 5% elongation in wet state is 0.54cN / dtex,

[0075] The dry elongation at break is 18.9%, and the wet elongation at break is 20.8%.

[0076] The crystallinity is 40%, the radial water swelling degree is 22.5%, and the matting agent content is 0.75%.

[0077] The whiteness is 84.6%, the linear density deviation rate is -10.0%, the residual sulfur is 8.0mg / 100g,

[0078] The length deviation rate is +10.0%, and the ultra-long fiber rate is 0.5%,

[0079] The double-length fiber is 4.0mg / 100g, and the defect is 4.0mg / 100g.

Embodiment 3

[0081] In order to better implement the present invention, this embodiment further provides the semi-dull high-strength low-elongation viscose fiber of the present invention and its preparation method, and measures the performance index.

[0082] Semi-dull high-strength low-elongation viscose fiber and its preparation method: the pulp raw material is soaked and pressed to remove the lye to obtain alkali cellulose; the prepared alkali cellulose is crushed, kneaded, and polymerized to remove the lye to obtain Methyl cellulose; the obtained methyl cellulose is yellowed to obtain cellulose sulfonate; the obtained cellulose sulfonate is dissolved in a solvent, filtered, matured, defoamed, and a spinning solution is obtained; After adding matting agent, the spinning solution is sent to spinning machine for spinning and drafting to obtain tow, and the tow is refined and dried to obtain viscose fiber of the present invention. Samples were taken, and each index was measured according t...

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Abstract

The invention provides semi-dull high-intensity low-elongation viscose fiber and a preparing method of the semi-dull high-intensity low-elongation viscose fiber. The viscose fiber is obtained through sequentially carrying out soaking, grinding, pressing and crushing, kneading, polymerization reduction, yellowing, dissolution, filtering, defoaming, aging, spinning traction and post treatment on pulp raw materials. The viscose fiber has the following indexes that the fiber number is 1.11 to 1.67 dtex, the dry fracture intensity is greater than or equal to 3.10cN / dtex, the wet fracture intensity is higher than or equal to 1.60cN / dtex, the intensity required for generating the 5-percent elongation rate in the wet state is higher than or equal to 0.55N / dtex, and the dry fracture elongation rate is 11.0 to 19.0 percent. The high-intensity low-elongation viscose fiber related by the invention is a novel fiber variety realized through technical innovation, an index system is different from that of ordinary viscose fiber and modal fiber; a product shows the high-intensity and low-elongation fiber features of the modal fiber, and also shows the higher skin affinity than cotton fiber; the existing differentiated viscose fiber can be effectively replaced; the downstream work procedure processing performance of the viscose fiber is improved; meanwhile, the development and the industrial updating of downstream novel textiles can also be promoted.

Description

technical field [0001] The invention relates to the technical field of viscose fiber, in particular to a semi-dull high-strength low-elongation viscose fiber and a preparation method thereof. Background technique [0002] Textile fiber raw materials are mainly divided into natural fiber raw materials represented by cotton and hemp, petroleum-based fiber raw materials represented by polyester and acrylic fibers, and tencel, cupro ammonia fiber, Viscose fiber and other bio-based fiber raw materials. Cotton fiber is well-known for its comfort, softness, breathability, and close-fitting qualities. It accounts for about 36% of the total textile fiber market. The nutritional content of cotton, and the reduction of cotton planting soil area in countries all over the world to ensure the food supply of the global population have limited the cultivation of cotton, and the shortage of cotton fiber raw materials cannot meet the growing needs of people's living standards. Viscose stapl...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F2/12D01D5/12D01D5/06D06M11/53D06M11/76D06L3/02D06L4/13
Inventor 冯涛邓传东李蓉玲贺敏黄艺陈明付李殿洪
Owner YIBIN GRACE GROUP CO LTD
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