Orange peel glycerol triacetate extract and application thereof in cigarettes

A technology of glycerol triacetate and extract, which is applied in the fields of application, tobacco, food science, etc., can solve the problems of cigarette difficulty, increased production cost, limited solubility of additives, complicated preparation process, etc., and achieve the reduction of smoke irritation, operation Strong and standardized, the effect of simple production process

Inactive Publication Date: 2015-09-30
CHINA TOBACCO YUNNAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

On the one hand, this method of adding and applying has the disadvantages of complex preparation process, limited solubility of triacetin for additives, and the difficulty of dissolving many additives that enhance flavor and sweetness of cigarettes into triacetin, which limits the Application in cigarette filter rod
On the other hand, if the filter rod is not flavored with triacetin as a medium, but the additive is directly applied to the cigarette filter rod, it will bring greater difficulty to cigarette production and significantly increase production costs, which is not conducive to large-scale production. Promoted application of

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] The orange peel is dried at 60°C until the water content is 10%, and then crushed into 20-40 mesh particles. Take by weight 300g orange peel particles and place them in a round bottom flask, add glycerol triacetate for tobacco with a solid-liquid ratio of 1:5 as an extractant, and carry out reflux extraction at 100°C for 8 hours. After being cooled to room temperature, the orange peel and glyceryl triacetate after reflux extraction are placed in an ultrasonic extractor (400W, 40kHZ), extracted for 25 minutes, and a clear solution is obtained after removing the filter residue by filtration, and the required orange peel triacetate can be obtained. Glyceryl acetate extract.

[0022] Using glyceryl triacetate as a solvent, the triacetin extract of orange peel is prepared into a solution with a concentration of 0.5%, and is evenly sprayed on the filter rod tow according to the ratio of 7% of the acetate fiber tow to make a cigarette filter rod. The cigarette whose filter ro...

Embodiment 2

[0024] The orange peel is dried at 80°C until the water content is 9%, and then crushed into 40-60 mesh particles. Take by weight 500g orange peel particles and place them in a round bottom flask, add glycerol triacetate for cigarettes with a solid-liquid ratio of 1:8 as an extractant, and carry out reflux extraction at 70°C for 15 hours. After being cooled to room temperature, the orange peel and glyceryl triacetate after reflux extraction are placed in an ultrasonic extractor (500W, 40kHZ), extracted for 35 minutes, and a clear solution is obtained after removing the filter residue by filtration, and the desired orange peel triacetate can be obtained. Glyceryl acetate extract.

[0025] Using glyceryl triacetate as a solvent, prepare a solution with a concentration of 1% of the extract of triacetin from orange peel, and spray evenly on the filter rod tow according to the weight of 7.5% of the acetate fiber tow to make a cigarette filter rod , through a conventional cigarette...

Embodiment 3

[0027] The orange peel is dried at 80°C until the water content is 8%, and then crushed into 20-60 mesh particles. Take by weight 600g orange peel particles and place them in a round bottom flask, add glycerol triacetate for cigarettes with a solid-liquid ratio of 1:10 as an extractant, and carry out reflux extraction at 120°C for 10 hours. After being cooled to room temperature, the orange peel and glyceryl triacetate after the reflux extraction are placed in an ultrasonic extractor (500W, 40kHZ), extracted for 45 minutes, and a clear solution is obtained after removing the filter residue by filtration, and the desired orange peel triacetate can be obtained. Glyceryl acetate extract.

[0028] Using glyceryl triacetate as a solvent, the orange peel triacetin extract is formulated into a solution with a concentration of 2%, and evenly sprayed on the filter rod tow according to the weight of 8% of the acetate fiber tow to make a cigarette filter rod. The cigarette whose filter ...

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PUM

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Abstract

The invention discloses an orange peel glycerol triacetate extract and application thereof in cigarettes. Orange peel particles with the moisture content of 8-10% and the grain size of 20-60 meshes serve as a raw material, glycerol triacetate serves as an extraction agent, and the orange peel glycerol triacetate extract is obtained first through extraction in a heating reflux mode and then through ultrasonic extraction. Glycerol triacetate serves as a solvent to prepare the orange peel glycerol triacetate extract into a solution with the concentration of 0.5-2%, the solution is evenly sprayed to tows according to the proportion of 6-8% of the weight of cellulose acetate tows to prepare a cigarette filter stick, and a cigarette with the filter stick containing effective orange peel components is prepared in the conventional cigarette winding process. The extract can remarkably enhance natural fragrance of the cigarette, enables the smoke to be fine and gentle and alleviates irritation and offensive odor, and the remaining taste is clean and comfortable. The orange peel glycerol triacetate extract is simple in production process and high in operability and normativity, raw materials can be obtained easily, the cost is low, industrial production is achieved conveniently, and the orange peel glycerol triacetate extract has good application prospect.

Description

technical field [0001] The invention belongs to the technical field of cigarette materials, and in particular relates to an orange peel triacetin extract. At the same time, the invention also relates to the application of the orange peel triacetin extract in cigarettes. Background technique [0002] Orange peel, also known as citrus peel, is pungent, slightly warm, and non-toxic. It has the effects of regulating qi and regulating the middle, drying dampness and eliminating phlegm, promoting qi and guiding stagnation. Orange peel is rich in sugars, citric acid, orange peel essential oil, natural pigments and flavonoids. Essential oils are mainly composed of terpenoids, higher alcohols, aldehydes, ketones, and esters. Citrus essential oil is a widely used additive, which is often used as tobacco essence in cigarettes and added to the liquid to participate in the combustion of cigarettes. In addition, it contains physiologically active ingredients such as hesperidin and hes...

Claims

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Application Information

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IPC IPC(8): A24B15/32A24B15/26C11B9/00
CPCA24B15/32A24B15/26C11B9/00
Inventor 陈剑明张天栋李勇朱龙田孟玉李万珣
Owner CHINA TOBACCO YUNNAN IND
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