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Chemical vapor deposition furnace and chemical vapor deposition system

A chemical vapor deposition, deposition chamber technology, applied in gaseous chemical plating, metal material coating process, coating and other directions, can solve the problems of chemical vapor deposition process termination, reduce product thickness, increase system blockage and other problems, to reduce dust The amount of staying in the deposition device, reducing the probability of clogging, and improving the effect of conversion rate

Inactive Publication Date: 2015-11-11
清远先导材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The chemical vapor deposition furnace used in the general chemical phase deposition system is basically a single deposition chamber. The chemical vapor deposition furnace with a single chamber is more convenient for small furnaces, but for a large number of industrial production, a single chamber The production cost of chemical vapor deposition furnace is relatively high, and it is inconvenient to operate
In addition, dust will be generated during the chemical vapor deposition process. If the dust cannot be properly and effectively treated, it will have a great impact on the performance of the product. In severe cases, it may lead to the termination of the entire chemical vapor deposition process.
[0005] Qingyuan Leading Materials Co., Ltd. applied for the patent "A Multi-chamber Graphite Deposition Device and Chemical Vapor Deposition Furnace" for the above problems, and proposed a solution to this problem. A dust collection mechanism is added above the deposition device in the deposition furnace, and the dust collection mechanism is provided with a dust collection container for collecting the dust escaping from the deposition chamber and for allowing the dust escaping from the deposition chamber to pass through and flow to the The dust collection channel of the dust collection container is described above. In the actual application process of the above chemical vapor deposition furnace, the added dust collection mechanism enables the dust generated during the chemical vapor deposition process to settle in the dust collection container when passing through the dust collection channel or after passing through. However, the above improvements increase the complexity of the chemical vapor deposition furnace of the deposition system, and at the same time, the products that are not deposited into the deposition chamber device enter the top of the deposition system device, increasing the probability of system blockage and reducing the deposition. The thickness of the product affects the performance of the product and reduces the conversion rate of the product

Method used

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Examples

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Embodiment 1

[0060] This embodiment provides a chemical vapor deposition system, including a chemical vapor deposition furnace, and the chemical vapor deposition furnace includes two deposition devices (2) and two raw material supply devices (1) corresponding to the two deposition devices , the two deposition devices (2) are arranged facing each other.

[0061] The raw material supply device comprises a graphite crucible (101) and a crucible base (102) made of isostatic graphite arranged under the graphite crucible (101).

[0062] The deposition device (2) is arranged above the raw material supply device (1), and the deposition device (2) is surrounded by four graphite deposition plates of the same size.

[0063] A first cover (6) is arranged between the raw material supply device (1) and the deposition device (2), and the first cover connects the cavity of the raw material supply device and the deposition device cavities separated. The first cover plate (6) is provided with a first raw ...

Embodiment 2

[0074] This embodiment provides a chemical vapor deposition system. The difference from Embodiment 1 is that the chemical vapor deposition furnace in the chemical vapor deposition system provided by this embodiment is provided with 4 deposition devices, and the 4 deposition devices are set correspondingly There are 4 crucibles. Wherein, the four deposition devices are evenly distributed around the center of the circle for 360°.

[0075] The thickness of zinc selenide produced by this method can reach 45mm, and the product conversion rate is 75%.

Embodiment 3

[0077] This embodiment provides a chemical vapor deposition system. The difference from Embodiment 1 is that the chemical vapor deposition furnace in the chemical vapor deposition system provided by this embodiment is provided with two deposition devices, and the two deposition devices are set correspondingly There are 2 crucibles. Wherein, the two deposition devices are evenly distributed in a circle around a central axis, the process gas is argon and the first raw material gas is hydrogen sulfide.

[0078] The thickness of zinc sulfide produced by this method can reach 44mm, and the product conversion rate is 69%.

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Abstract

The invention provides a chemical vapor deposition furnace comprising a material supplying device, two or more deposition devices and a collecting device. The material supplying device is used for containing solid raw materials and supplying gaseous state raw materials to the deposition chamber. The deposition devices are arranged above the raw material supplying device. The material collecting device is arranged above the deposition devices. The collecting device comprises a collecting box, a collecting box cover arranged on the top of the collecting box and an air outlet cylinder formed in the collecting box cover. The collecting box is an internally through cavity. The lower end of the air outlet cylinder is communicated with the cavity of the collecting box. According to the chemical vapor deposition furnace, unreacted gas and future and deposited compound particles directly enter the collecting box and enter a dust collecting system connected with the chemical vapor deposition furnace as much as possible, so that the load borne by the whole chemical vapor deposition furnace is lowered; meanwhile, the amount of dust generated due to a reaction and staying in the deposition device is reduced, and the possibility of blockage of the system is lowered; and correspondingly, the thickness of products is increased, and the conversion rate of products is increased.

Description

technical field [0001] The invention belongs to the technical field of chemical vapor deposition, and in particular relates to a chemical vapor deposition furnace and a chemical vapor deposition system. Background technique [0002] Chemical vapor deposition (Chemical vapor deposition, referred to as CVD) is a new technology for the preparation of inorganic materials developed in recent decades. Chemical vapor deposition is a process technology in which two or more gaseous substances react chemically on a substrate under vacuum conditions to form a solid substance that is deposited on the surface of the substrate to obtain a solid material. Chemical vapor deposition has been widely used to purify substances, develop new crystals, deposit various single crystal, polycrystalline or glassy inorganic thin film materials, infrared materials, etc. [0003] The chemical vapor deposition system includes a chemical vapor deposition furnace, a gas delivery system that provides gas to...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C16/44C23C16/455
Inventor 朱刘于金凤
Owner 清远先导材料有限公司