A wood-plastic composite material board with cross-linked microporous structure and preparation method thereof
A technology of wood-plastic composite material and microporous structure, which is applied in the field of wood-plastic composite material with cross-linked microporous structure and its preparation, and can solve the problems of reduced ductility and impact resistance, limited wide use, and high material brittleness. problem, to achieve the effect of reducing the amount of plastic, not easy to age and change color, and strong wood feeling
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Embodiment 1
[0039] Polyvinyl chloride plastic particles 100kg, acrylic modified wood powder (particle size 100 mesh) 30kg,
[0040] Benzoic acid 0.2kg, POE-g-MAH (grafting rate 0.8%) 3kg,
[0041] PET fiber (length 3.5mm) 3kg, bis-tert-butyl peroxide cumene 0.2kg,
[0042] Azodicarbonamide 4kg, compound auxiliary blowing agent 4kg,
[0043] Triallyl isocyanurate 5kg, tribasic lead sulfate 6kg,
[0044] Dibutyl phthalate 1.1kg,
[0045] A kind of preparation method of the wood-plastic composite board material with cross-linked microporous structure of the present invention, it comprises the following steps:
[0046] (1) Weigh dichloromethane, acrylic acid, carbonyldiimidazole and wood flour at a mass ratio of 100:15:30:30, dissolve acrylic acid in dichloromethane to form an acrylic acid solution, raise the temperature of the solution to 45°C, and then Add carbonyldiimidazole dropwise to the acrylic acid solution for 45 minutes. After the dropwise addition is complete, continue the reac...
Embodiment 2
[0051] Polyvinyl chloride plastic particles 100kg, acrylic modified wood powder (particle size 80 mesh) 20kg,
[0052] Benzoic acid 0.1kg, POE-g-MAH (grafting rate 0.7%) 2kg,
[0053] PET fiber (length 1mm) 1kg, bis-tert-butyl peroxide cumene 0.1kg,
[0054] Azodicarbonamide 3kg, compound auxiliary blowing agent 2kg,
[0055] Triallyl isocyanurate 2kg, tribasic lead sulfate 4kg,
[0056] Dibutyl phthalate 0.6kg,
[0057] A kind of preparation method of the wood-plastic composite board material with cross-linked microporous structure of the present invention, it comprises the following steps:
[0058] (1) Weigh dichloromethane, acrylic acid, carbonyldiimidazole and wood flour in a mass ratio of 100:10:20:10, dissolve acrylic acid in dichloromethane to form an acrylic acid solution, raise the temperature of the solution to 40°C, and then Add carbonyldiimidazole dropwise to the acrylic acid solution for 30 minutes. After the dropwise addition is complete, continue the reactio...
Embodiment 3
[0063] Polyvinyl chloride plastic particles 100kg, acrylic modified wood flour (particle size 120 mesh) 40kg,
[0064] Benzoic acid 0.3kg, POE-g-MAH (grafting rate 0.9%) 4kg,
[0065] PET fiber (length 6mm) 6kg, bis-tert-butyl peroxide cumene 0.3kg,
[0066] Azodicarbonamide 5kg, compound auxiliary blowing agent 6kg,
[0067] Triallyl isocyanurate 8kg, tribasic lead sulfate 8kg,
[0068] Dibutyl phthalate 1.6kg,
[0069] A kind of preparation method of the wood-plastic composite board material with cross-linked microporous structure of the present invention, it comprises the following steps:
[0070] (1) Weigh dichloromethane, acrylic acid, carbonyldiimidazole and wood flour in a mass ratio of 100:20:40:50, dissolve acrylic acid in dichloromethane to form an acrylic acid solution, raise the temperature of the solution to 50°C, and then Add carbonyldiimidazole dropwise to the acrylic acid solution for 60 minutes. After the dropwise addition is complete, continue the reactio...
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