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631results about How to "Won't release" patented technology

High-early strength antifreezing polycarboxylate high performance water reducing agent and preparation

The invention discloses an early-strength antifreezing polycarboxylate high-performance water reducing agent and a method for preparing the same. The early-strength antifreezing water reducing agent is prepared from a polycarboxylate water reducing agent, an early-strength antifreezing agent, an air entraining agent and water. The method comprises the following steps: A, the synthesis of the polycarboxylate high-performance water reducing agent: (1) esterification reaction; adding methacrylic acid, and the like to a reaction kettle, and (2) polymerization reaction; heating big monomer methoxy polyethyleneglycol methacrylic ester; B, the preparation for the solution of an early-strength antifreezing agent: a, weighing water and adding the same to the reaction kettle, and adding calcium formate to the reaction kettle, and b, adding triethanolamine, and the like to the reaction kettle to prepare the early-strength antifreezing agent solution; C, the preparation of the air entraining agent: weighing water and adding the same to the reaction kettle, and adding powdered three-level colophony to the reaction kettle to obtain the air entraining agent; and D, the preparation of the finished product: weighing the polycarboxylate water reducing agent and adding the same to the reaction kettle, and adding the air entraining agent and the early-strength antifreezing agent solution to the reaction kettle. The early-strength antifreezing polycarboxylate high-performance water reducing agent has higher water reducing rate and remarkable enhancing effect, and is suitable to prepare various common concrete and high-performance concrete at a negative temperature range of between 20 DEG C below zero and 0 DEG C.
Owner:武汉市联合石油化工有限责任公司

Method for preparing graphene oxide modified composite phase-change microcapsule

The invention discloses a method for preparing graphene oxide modified composite phase-change microcapsules. The method specifically comprises the following steps: preparing a graphene oxide solid from graphite powder, concentrated sulfuric acid, sodium nitrate, potassium permanganate and deionized water; mixing the obtained graphene oxide solid with absolute ethyl alcohol and a silane coupling agent, and performing a reaction so as to obtain a double-bond modified functional graphene oxide solid; uniformly mixing the obtained functional graphene oxide solid with a phase-change material, a reaction monomer, a cross-linking agent, a reactive emulsifier and deionized water, and performing ultrasonic dispersion so as to form an oil-in-water type pre-emulsion; and putting the obtained oil-in-water type pre-emulsion into a hot water bath, continuously stirring, further adding an initiator solution, and performing a heat-preservation reaction, thereby obtaining the graphene oxide modified composite phase-change microcapsules. By adopting the method disclosed by the invention, composite phase-change microcapsules which are high in encapsulation efficiency, stable in property, good in heat conductivity, appropriate in phase-change temperature and relatively high in phase-change latent heat enthalpy can be prepared.
Owner:SHAANXI UNIV OF SCI & TECH

Compound microbial preparation for treating black and odorous rivers through strengthened calcium nitrate

The invention relates to a compound microbial preparation for treating black and odorous rivers through strengthened calcium nitrate and a preparation method thereof. The use amount of calcium nitrate is reduced, and the time for treating the black and odorous rivers is shortened. The compound microbial preparation is prepared from 40-80 parts of thiobacillus denitrificans and thiocapsa roseoppersicina mixed powder, 10-60 parts of composite bacillus subtilis powder and 10-60 parts of yeast and lactic acid bacterium mixed powder. By means of the preparation, sulfide in black and odorous bottom sludge, organic matter and strains suitable for growing in the black and odorous bottom sludge are screened and degraded in a targeted mode; by means of thiobacillus denitrificans with efficient hydrogen sulfide degrading and denitrification capacity, sulfur-oxidizing bacteria of thiocapsa roseoppersicina with efficient hydrogen sulfide and ammoniacal nitrogen degrading capacity, bacilli rich in protease, amylase, cellulose and other enzyme systems, yeast and lactic acid bacteria, a small amount of calcium nitrate and the compound microbial preparation are thrown into the black and odorous rivers so that water quality of the black and odorous rivers can be quickly improved, the black and odorous bottom sludge can be removed quickly, and the thickness and the organic matter content of the bottom sludge can be quickly reduced.
Owner:胡艳晖

Low-smoke, halogen-free and flame-retardant thermoplastic polyolefin elastomer composite with ceramization function as well as preparation method and application thereof

The invention relates to the technical field of polyolefin elastomers, in particular to a low-smoke, halogen-free and flame-retardant thermoplastic polyolefin elastomer composite with a ceramization function as well as a preparation method and an application thereof. The low-smoke, halogen-free and flame-retardant ceramic thermoplastic polyolefin elastomer composite is prepared from raw materials in parts by weight as follows: 20-80 parts of thermoplastic polyolefin, 2-10 parts of EVA (ethylene-vinyl acetate) resin, 2-10 parts of ethylene propylene rubber, 20-70 parts of a halogen-free flame retardant, 1-10 parts of a smoke suppressant, 20-80 parts of ceramization powder, 0.5-5 parts of a compatilizer and 0.02-0.1 parts of an antioxidant. The low-smoke, halogen-free and flame-retardant ceramic thermoplastic polyolefin elastomer composite has a good flame retardant effect and is low in smoke density, high in strength, good in flexibility and high in elongation at break; a compact ceramization product can be formed at the temperature of 600-1,000 DEG C, the ceramization temperature is low, ceramization is compact, and the formed ceramization product has good high-temperature strength and heat flow impact resistance.
Owner:ADVANCED THERMOPLASTIC POLYMER TECH

Halogen-free flam retardant prepolymer, preparation method thereof and application of halogen-free flam retardant prepolymer in copper clad laminate (CCL)

The invention particularly relates to a halogen-free flame retardant prepolymer, and an application thereof in the manufacture of the copper clad laminate (CCL). The manufacture of the CCL comprises the following steps: taking and reacting the bismaleimides, allyl compound and phosphorus-containing compound for 10 to 120 minutes at the temperature of 80 to 160 DEG C to obtain the halogen-free flame retardant prepolymer; preparing the prepolymer into solution, stirring uniformly the solution to obtain a glue solution, coating the glue solution uniformly on an E-glass fiber cloth with smooth surface, and then baking the E-glass fiber cloth to prepare a B-rank prepreg; and cutting the B-rank prepreg into proper size according to the size of a pressing machine, overlapping a certain amount of prepregs, and pressing the prepregs with a copper foil with the same size on the top and a copper foil with the same size at the bottom in a hot pressing machine to obtain the CCL. The CCL has good flame retardant effect, no release of harmful gases during the burning, and the product after the solidification of the CCL has the advantages of good toughness, higher thermal decomposition temperature and lower dielectric loss.
Owner:SHENGYI TECH SUZHOU

Combined type machine set integrating functions of banburying, feeding and extruding into whole

The invention discloses a combined type machine set integrating the functions of banburying, feeding and extruding into a whole, which comprises a rack divided into two layers, wherein the top layer of the rack is provided with a banbury mixer. The combined type machine set is characterized in that the bottom layer of the rack is provided with a single-screw extrusion machine and a conical double-screw feeding machine, wherein a feed inlet is arranged above a machine barrel of the conical double-screw feeding machine, a feeding hopper is installed at the feed inlet, an outlet of a discharge device of the banbury mixer is positioned above the feeding hopper and can discharge materials to the feeding hopper, and double screws of the conical double-screw feeding machine are connected with a feed inlet at one side of the machine barrel of the single-screw extrusion machine. The invention solves the problems that a plastic granulation manufacturing procedure in the prior art is complicated, has low working efficiency and wastes a large amount of manpower, material resources and space, provides the combined type machine set integrating the functions of banburying, feeding and extruding into a whole, saves the working time greatly, enhances the working efficiency and saves the enterprise cost.
Owner:KUSN KESUN RUBBER & PLASTIC MACHINERY

Powder evanescent mode casting paint and application method and application thereof

InactiveCN106694798AGood bonding performance at room temperatureImprove breathabilityFoundry mouldsFoundry coresPhosphatePolyvinyl alcohol
The invention discloses powder evanescent mode casting paint and an application method thereof. The powder paint comprises the following components in percentage by weight: 88.9-89.7% of refractory aggregate, 3.7-4.5% of sodium base bentonite, 0.78-1.23% of polyethyl alcohol, 0.82-1.85% of aluminum dihydrogen phosphate, 0.32-0.44% of sodium carboxymethylcellulose, and 3.8-4.8% of expanded graphite. During preparing, all powder is added in a mixer for dry mixing to reach an uniform state to obtain the finished powder evanescent mode casting paint. Water by 23.5-37 weight% of the powder paint is firstly added in the mixer; the mixer is started; the powder paint is slowly added in the mixer; after materials are added, the stirring is continued by 1-2 hours; and then, an evanescent mode can be coated by the paint. The paint can achieve the effect of long-time storage without deteriorating by adding no formaldehyde in the raw materials; no surface active agent is added in the raw materials to prevent the trouble of adding a defoaming agent to defoam in subsequent use; the finished product is higher in strength at normal temperature or high temperature; and the paint is excellent in permeability, and cannot release poisonous substances.
Owner:HUBEI UNIV OF TECH

Preparation method of fire retardant coating

The invention relates to a preparation method of a fire retardant coating. The preparation method comprises the following steps of: firstly, mixing polyalcohol, ammonium polyphosphate and montmorillonite for stirring; adding diisocyanate, dimethylolpropionic acid and a catalyst into the obtained mixture; after reaction, obtaining a prepolymer; adding 1, 4-butanediol into the prepolymer, carrying out reaction and obtaining a neutral body; cooling the neutral body and then adding triethylamine into the cooled neutral body for reaction; adding nano-microcrystalline cellulose water solution treated by dispersion into the reaction product, stirring and obtaining emulsion; and transferring the emulsion into a template, molding and obtaining the fire retardant coating. According to the method, polyurethane is taken as a film forming matter, the nano-microcrystalline cellulose is taken as a carbonizing agent, the ammonium polyphosphate is taken as an acid source and a gas source, and the montmorillonite has the reinforcement function. The fire retardant coating prepared by the invention is free from pollution, is safe and reliable, is good in mechanical performance, and does not emit corrosive gases such as hydrogen halide and the like when being decomposed by heating.
Owner:NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI

Large power thick film circuit high temperature sintering resistor paste for aluminium nitride base materials, and preparation method thereof

The invention discloses a large power thick film circuit high temperature sintering resistor paste for aluminium nitride base materials, and a preparation method thereof. The thick film resistor paste includes an inorganic bonding phase, a composite function phase, and an organic carrier, wherein an inorganic bonding phase is formed by SiO2, B2O3, ZnO, Al2O3, MgO, nucleus agent, and rare earth oxide system microcrystalline glass powder; the composite function phase is mixed powder of spherical silver powder, sheet shape silver powder, and nanometer palladium powder; and the organic carrier is formed by organic solvent, high-molecular thickening agent, dispersant, antifoaming agent and thixotropic agent. The preparation method comprises the steps: inorganic bonding phase preparation, composite function phase preparation, organic carrier preparation and resistor paste preparation. The paste has high thixotropy and fluidity, and the microcrystalline glass powder and the conductive phase do not react with the aluminium nitride base materials, and the sintered resistance layer has the advantages of being smooth and compact in structure, being high in adhesive force, being aging resistant, being adjustable in sheet resistivity, being lower and adjustable in the resistance temperature coefficient and being high in printing sintering characteristic.
Owner:DONGGUAN COREHELM ELECTRONICS MATERIAL TECH CO LTD
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