Novel modified cotton fiber for infants based on liquid freezing and preparation process thereof
A preparation process, infant technology, applied in fiber processing, plant fibers, textiles and papermaking, etc., can solve the problem of moisture absorption decline, achieve the effect of improving anti-wrinkle performance, facilitating refinement, and improving durability
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Embodiment 1
[0027] (1) After the cotton fibers are removed from the surface impurities, they are immersed in deionized water, taken out and aired to obtain cotton fibers with a moisture content of 20%, and the moisture-containing cotton fibers are placed in a subzero-10°C environment to freeze to obtain pretreated cotton fibers. fiber.
[0028] (2) Put the pretreated cotton fiber prepared in step (1) into the sarong of the liquid ammonia treatment tank, vacuumize, and process 2 times through intermittent and repeated liquid ammonia treatment, wherein the intermittent and repeated liquid ammonia treatment includes dispensing a sufficient amount of liquid ammonia Immerse the cotton fiber for 10s, drain the ammonia and pump out the ammonia gas, and remove the ammonia by microwave for 3min at a power of 50kW to obtain the cotton fiber treated by liquid freezing.
[0029] (3) the cotton fiber of the liquid freezing treatment that step (2) is prepared is placed in the chitosan treatment liquid ...
Embodiment 2
[0030] (1) After the cotton fibers are removed from the surface impurities, they are immersed in deionized water, taken out and aired to obtain cotton fibers with a moisture content of 60%, and the hydrated cotton fibers are placed in a subzero-20°C environment to freeze to obtain pretreated cotton fibers. fiber.
[0031] (2) Put the pretreated cotton fiber prepared in step (1) into the sarong of the liquid ammonia treatment tank, vacuumize, and process 3 times through intermittent and repeated liquid ammonia treatment, wherein the intermittent and repeated liquid ammonia treatment includes dispensing a sufficient amount of liquid ammonia Immerse the cotton fiber for 20s, drain the ammonia and pump the ammonia gas, and remove the ammonia by microwave at 80kW power for 5min to obtain the cotton fiber treated by liquid freezing.
[0032] (3) the cotton fiber of the liquid freezing treatment that step (2) is prepared is placed in the chitosan treatment liquid with a bath ratio of...
Embodiment 3
[0034] (1) After the cotton fibers are removed from the surface impurities, they are immersed in deionized water, taken out and dried to obtain cotton fibers with a moisture content of 50%, and the hydrated cotton fibers are placed in a subzero-15°C environment to freeze to obtain pretreated cotton fibers. fiber.
[0035] (2) Put the pretreated cotton fiber prepared in step (1) into the sarong of the liquid ammonia treatment tank, vacuumize, and process 2 times through intermittent and repeated liquid ammonia treatment, wherein the intermittent and repeated liquid ammonia treatment includes dispensing a sufficient amount of liquid ammonia Immerse the cotton fibers for 15s, drain the ammonia and pump out the ammonia gas, and remove the ammonia by microwave at 60kW power for 4min to obtain the cotton fibers treated by liquid freezing.
[0036] (3) the cotton fiber of the liquid freezing treatment that step (2) is prepared is placed in the chitosan treatment liquid with a bath ra...
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