A process of printing and dyeing leather with lemon peel juice
A technology of lemon peel and leather, applied in the field of leather dyeing, to achieve natural color, achieve dyeing balance, and improve the effect of dyeing quality
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Embodiment 1
[0048] The process of printing and dyeing leather with lemon peel juice, the process includes the following steps:
[0049] 1) extract lemon yellow pigment:
[0050] Extraction: Remove the pulp from fresh lemons, scrape off the peels, chop them and add NaCl to marinate for 1 hour, then transfer them to the extractor, add 90% ethanol to extract at 50°C for 2.5 hours, and the extraction is over Finally, ethanol is recovered to obtain a tartrazine concentrated solution;
[0051]Purification: Put the above-mentioned lemon yellow pigment concentrate on a silica gel column, and use a mixture of oil ether and 90% ethanol as the eluent to elute, wherein the volume ratio of petroleum ether and ethanol is 2:1; collect the yellow eluate part, depressurize Concentrate to obtain purified lemon yellow pigment;
[0052] 2) Dye preparation:
[0053] Add tartrazine extract and color-fixing agent to the lemon yellow pigment obtained in step 1), wherein 37 parts of lemon yellow pigment, 12 pa...
Embodiment 2
[0059] The process of printing and dyeing leather with lemon peel juice, the process includes the following steps:
[0060] 1) extract lemon yellow pigment:
[0061] Extraction: Fresh lemons are peeled and peeled after the pulp is removed, chopped and marinated with NaCl for 1.5 hours, then transferred to the extractor, added with 92% ethanol to extract at 65°C for 2 hours, and the extraction is completed Finally, ethanol is recovered to obtain a tartrazine concentrated solution;
[0062] Purification: Put the above-mentioned lemon yellow pigment concentrate on a silica gel column, and use a mixture of oil ether and 90% ethanol as the eluent to elute, wherein the volume ratio of petroleum ether and ethanol is 2:1; collect the yellow eluate part, depressurize Concentrate to obtain purified lemon yellow pigment;
[0063] 2) Dye preparation:
[0064] Add tartrazine extract and color-fixing agent to the lemon yellow pigment obtained in step 1), wherein 46 parts of lemon yellow ...
Embodiment 3
[0070] The process of printing and dyeing leather with lemon peel juice, the process includes the following steps:
[0071] 1) extract lemon yellow pigment:
[0072] Extraction: Remove the pulp from fresh lemons, scrape off the peels, chop them and add NaCl to marinate for 2 hours, then transfer them to the extractor, add 95% ethanol to extract at 80°C for 1.5 hours, and the extraction is over Finally, ethanol is recovered to obtain a tartrazine concentrated solution;
[0073] Purification: Put the above-mentioned lemon yellow pigment concentrate on a silica gel column, and use a mixture of oil ether and 90% ethanol as the eluent to elute, wherein the volume ratio of petroleum ether and ethanol is 2:1; collect the yellow eluate part, depressurize Concentrate to obtain purified lemon yellow pigment;
[0074] 2) Dye preparation:
[0075] Add tartrazine extract and color-fixing agent to the lemon yellow pigment obtained in step 1), wherein 62 parts of lemon yellow pigment, 25 ...
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