A kind of antibacterial and antifungal agent and preparation method thereof and antibacterial and antifungal method
An antibacterial and antifungal agent and antifungal technology, applied in the field of antibacterial, can solve the problems of low antibacterial and antifungal performance, low production cost and high production cost, and achieve the effects of low production cost, reduced toxicity and improved aging.
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Embodiment 1
[0029] (1) Weigh the following raw materials: 0.5gAgNO 3 , 20g nano-ZnO, 60g calcined diatomite, 15gN-octyl-4-isothiazolin-3-one, wherein the particle size of nano-ZnO is 20nm; the AgNO 3 Prepare a solution with a molar concentration of 0.5mol / L, and then calcined diatomite and AgNO 3 The solutions are mixed, stirred, and the pH value of the mixed solution is adjusted to 5, the temperature of the mixed solution is 50°C during stirring, and the stirring time is 2 hours, and then the mixed solution is centrifuged, filtered and dehydrated to obtain the first solid;
[0030] (2) N-octyl-4-isothiazolin-3-one is formulated into a solution with a mass fraction of 20%, the above-mentioned first solid is added to the solution and mixed, fully stirred and the pH value of the mixed solution is adjusted to 6, to obtain the first mixed solution;
[0031] (3) adding nano-ZnO to the above-mentioned first mixed solution, stirring at a rotating speed of 1500r / min for 2h to obtain a second mi...
Embodiment 2
[0038] (1) Weigh the following raw materials: 3gCuSO 4 , 20g nano-TiO 2 , 32g nano-ZnO, 65g first-grade diatomite, 10g benzoimidazole methyl carbamate, of which nano-TiO 2 and nano-ZnO particle size are 30nm; the CuSO 4 Prepare a solution with a molar concentration of 3mol / L, and then mix the primary diatomite and CuSO 4 The solutions are mixed, stirred, and the pH value of the mixed solution is adjusted to 8, the temperature of the mixed solution is 40°C during stirring, and the stirring time is 10 hours, and then the mixed solution is centrifuged, filtered and dehydrated to obtain the first solid;
[0039] (2) Methyl benzoimidazole carbamate is formulated into a solution with a mass fraction of 30%, the above-mentioned first solid is added to the solution and mixed, fully stirred and the pH value of the mixed solution is adjusted to 8 to obtain the first mixed solution liquid;
[0040] (3) Nano-TiO 2and nano-ZnO were added to the above-mentioned first mixed solution, an...
Embodiment 3
[0044] (1) Weigh the following raw materials: 5gCu(NO 3 ) 2 , 40g nano-TiO 2 , 62g of secondary diatomite, 10g of iodopropynyl butyl carbamate, of which nano-TiO 2 The particle size is 20nm; the Cu(NO 3 ) 2 Prepare a solution with a molar concentration of 5mol / L, and then mix the secondary diatomite and Cu(NO 3 ) 2 The solution is mixed, stirred and the pH value of the mixed solution is adjusted to 7, the temperature of the mixed solution is 80° C. during stirring, the stirring time is 7 hours, and then the mixed solution is centrifuged, filtered and dehydrated to obtain the first solid;
[0045] (2) Iodopropynyl butyl carbamate is formulated into a solution with a mass fraction of 30%, the above-mentioned first solid is added to the solution and mixed, fully stirred and the pH value of the mixed solution is adjusted to 5 to obtain the second a mixture;
[0046] (3) Nano-TiO 2 Add it into the first mixed solution above, and stir for 3 hours at a speed of 1500r / min to o...
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