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A kind of ultra-high strength nanocrystalline al-mg aluminum alloy material and preparation method thereof

An aluminum alloy material and nanocrystalline technology, which is applied in the field of ultra-high strength nanocrystalline Al-Mg aluminum alloy material and its preparation, can solve the problems of low strength and low manufacturing cost, and achieve the goal of increasing strength, reducing energy consumption, and reducing costs Effect

Active Publication Date: 2018-04-24
JIANGSU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] The purpose of the present invention is to overcome the deficiencies of the prior art, aiming at the problem of low strength of the existing 5000 series Al-Mg aluminum alloys, to provide an ultra-high-strength nanocrystalline Al-Mg aluminum alloy material and a preparation method thereof. The combination of design and high-pressure torsion refines the grains of Al-Mg aluminum alloys to a nanoscale of less than 100nm, and obtains high-density dislocations and high-density nanoscale stacking faults in the alloy, using strong fine-grain strengthening, Strengthening mechanisms such as dislocation strengthening and nanoscale stacking fault strengthening greatly increase the strength of the alloy, expanding the application range of 5000 series Al-Mg aluminum alloys. The preparation method of this method is simple and the manufacturing cost is lower than the existing preparation methods.

Method used

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  • A kind of ultra-high strength nanocrystalline al-mg aluminum alloy material and preparation method thereof
  • A kind of ultra-high strength nanocrystalline al-mg aluminum alloy material and preparation method thereof
  • A kind of ultra-high strength nanocrystalline al-mg aluminum alloy material and preparation method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0051] Cast the Al-6.0Mg aluminum alloy into a circular billet with a diameter of 50mm, and process it into a disc with a size of Φ20×2mm by turning. The disc is homogenized at 450°C×2h in a circulating air resistance furnace , and then perform high-pressure torsion on the homogenized disc, the process of high-pressure torsion is: torsion 10 circles under the process conditions of room temperature, pressure 6GPa, and rotational speed 1r / min. The aluminum alloys twisted under high pressure at room temperature were then subjected to the average grain size determination, hardness measurement and tensile test.

[0052] The test results of the above-mentioned Al-6.0Mg aluminum alloy twisted at room temperature and high pressure for 10 turns are shown in Table 2 and Figure 5 , the average grain size of the prepared alloy is d TEM is 68nm, the hardness HV is 2061MPa, and the tensile strength σ b 845MPa, yield strength σ 0.2 It is 845MPa.

Embodiment 2

[0057] Cast the Al-8.0Mg aluminum alloy into a circular billet with a diameter of 50mm, and process it into a disc with a size of Φ20×2mm by turning. The disc is homogenized at 450°C×2h in a circulating air resistance furnace , and then perform high-pressure torsion on the homogenized disc, the process of high-pressure torsion is: torsion 10 circles under the process conditions of room temperature, pressure 6GPa, and rotational speed 1r / min. The aluminum alloys twisted under high pressure at room temperature were then subjected to the average grain size determination, hardness measurement and tensile test.

[0058] The test results of the above-mentioned Al-8.0Mg aluminum alloy twisted at room temperature and high pressure for 10 turns are shown in Table 2 and Figure 6 , the average grain size of the prepared alloy is d TEM 65nm, hardness HV is 2141MPa, tensile strength σ b 855MPa, yield strength σ 0.2 It is 830MPa.

Embodiment 3

[0063] Cast the Al-10.0Mg aluminum alloy into a circular billet with a diameter of 50mm, and process it into a disc with a size of Φ20×2mm by turning. The disc is homogenized at 450°C×2h in a circulating air resistance furnace , and then perform high-pressure torsion on the homogenized disc, the process of high-pressure torsion is: torsion 10 circles under the process conditions of room temperature, pressure 6GPa, and rotational speed 1r / min. The aluminum alloys twisted under high pressure at room temperature were then subjected to the average grain size determination, hardness measurement and tensile test.

[0064] The test results of the above-mentioned Al-10.0Mg aluminum alloy twisted at room temperature and high pressure for 10 turns are shown in Table 2 and Figure 7 , the average grain size of the prepared alloy is d TEM is 57nm, the hardness HV is 2396MPa, and the tensile strength σ b 795MPa, yield strength σ 0.2 It is 795MPa.

[0065] The average grain size and mec...

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Abstract

The invention provides an ultrahigh-strength nanocrystalline Al-Mg aluminum alloy material and a preparation method thereof, belonging to the technical field of preparation of metals and alloys. The composition and weight percentage of the alloy are: 6.0‑10.0% Mg, the rest are Al and impurity elements, and the impurity elements are Si<0.06%, Fe<0.08%, and Ti<0.05%. In the method, the aluminum alloy is firstly cast to form an as-cast billet, and then the as-cast billet is turned into a high-pressure torsion disk and then homogenized; and then the homogenized disk is subjected to high-pressure torsion at room temperature for 1 to 10 turns. The Al-Mg aluminum alloy material prepared by the method provided by the invention has a grain size of 57-68 nm, a tensile strength of 800-855 MPa, and a yield strength of 795-845 MPa. Compared with the usual medium-strength 5000-series aluminum alloy, the strength of the nanocrystalline Al-Mg aluminum alloy material of the present invention is greatly improved, reaching the level of super-strength aluminum alloy, and the production efficiency is higher and the cost is lower, expanding the range of 5000-series aluminum The scope of application of the alloy.

Description

technical field [0001] The invention belongs to the technical field of metal and alloy preparation, and relates to an ultrahigh-strength nanocrystalline Al-Mg aluminum alloy material and a preparation method thereof. Background technique [0002] As an important non-heat-treatable alloy, the 5000 series Al-Mg alloy has good corrosion resistance, formability, weldability and medium strength, and is so far used in low-temperature storage tanks, aluminum wall panels, lighting products, and memory disk substrates. , marine engine parts, plates for large ships, outer panels of military armored vehicles, tank floors, interior panels of automobile bodies, etc., are the most widely used aluminum alloy materials. The strength and other mechanical properties of alloys can no longer meet the practical application, and it is urgent to improve the comprehensive mechanical properties of alloys. [0003] At present, improving the strength of 5000 series Al-Mg aluminum alloys has become a ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C21/06C22C21/08C22C1/02C22C1/06C22F1/047
Inventor 刘满平程晓农刘强张振亚孙少纯
Owner JIANGSU UNIV