Polyhedral cobalt phosphide/graphite carbon hybrid material and its preparation method and application
A hybrid material, cobalt phosphide technology, used in materials and energy fields, can solve the problems of large size of phosphide, easy agglomeration, reduced catalytic activity and stability, etc., and achieve large specific surface area, high catalytic activity and low cost. Effect
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Embodiment 1
[0017] Embodiment 1, polyhedral cobalt phosphide / graphite carbon hybrid material and its preparation method and application, comprises the following steps:
[0018] (1) Preparation of ZIF-67 template with polyhedral morphology: Weigh 1.46 g of cobalt nitrate hexahydrate and 1.64 g of 2-methylimidazole, dissolve them in 80 ml of methanol and ethanol mixed solution, stir and dissolve, and The cobalt nitrate solution was poured into the 2-methylimidazole solution. After stirring for 5 minutes, stand at room temperature for 24 hours, centrifuge the product, wash it twice with ethanol solution, and finally place it in a 60-degree drying oven. The obtained product is polyhedral ZIF-67. The product is blue-purple, mostly rhomboid dodecahedron in shape, and the particle size is about 1 micron.
[0019] (2) Polyhedral cobalt phosphide / graphite carbon hybrid material and its preparation: Weigh 200 mg of ZIF-67 and 200 mg of red phosphorus and place them on both ends of the porcelain bo...
Embodiment 2
[0022] Embodiment 2, the preparation method of polyhedral cobalt phosphide / graphite carbon hybrid material, comprises the following steps:
[0023] (1) Preparation of ZIF-67 template with polyhedral morphology: Weigh 1.46 g of cobalt nitrate hexahydrate and 1.64 g of 2-methylimidazole, dissolve them in 150 ml of methanol and ethanol mixed solution, stir and dissolve, and The cobalt nitrate solution was poured into the 2-methylimidazole solution. After stirring for 1 minute, stand at room temperature for 24 hours, centrifuge the product, wash twice with ethanol solution, and finally place it in a 60-degree drying oven. The obtained product is polyhedral ZIF-67. The product is blue-purple in shape, mostly in the shape of rhombic dodecahedron, and the particle size is between 1 and 2 microns.
[0024] (2) Polyhedral cobalt phosphide / graphite carbon hybrid material and its preparation: Weigh 200 mg of ZIF-67 and 200 mg of red phosphorus and place them on both ends of the porcelai...
Embodiment 3
[0027] Embodiment 3, the preparation method of polyhedral cobalt phosphide / graphite carbon hybrid material, comprises the following steps:
[0028] (1) Preparation of ZIF-67 template with polyhedral morphology: Weigh 1.46 g of cobalt nitrate hexahydrate and 1.64 g of 2-methylimidazole, dissolve them in 200 ml of methanol and ethanol mixed solution, stir and dissolve, and The cobalt nitrate solution was poured into the 2-methylimidazole solution. After stirring for 5 minutes, stand at room temperature for 24 hours, centrifuge the product, wash it twice with ethanol solution, and finally place it in a 60-degree drying oven. The obtained product is polyhedral ZIF-67. The product is blue-purple, mostly rhomboid dodecahedron in shape, and the particle size is about 3 microns.
[0029] (2) Polyhedral cobalt phosphide / graphite carbon hybrid material and its preparation: Weigh 200 mg of ZIF-67 and 200 mg of red phosphorus and place them on both ends of the porcelain boat respectively...
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