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56results about How to "Good ball" patented technology

Film-coated modified propping agent, and preparation method and application thereof

The invention discloses a film-coated modified propping agent, and a preparation method and an application thereof. The film-coated modified propping agent is composed of a matrix and a resin layer uniformly coated out of the matrix, wherein the matrix is Hobq quartz sand; the resin layer is 1-10 wt% based on that of the matrix; and the resin layer comprises a resin binder and a curing agent, wherein the resin binder is bisphenol A epoxy resin, polyurethane resin or a combination thereof, the curing agent is an aliphatic polyamine curing agent an oralicyclic amine curing agent, and the usage amount of the curing agent is 10-50 wt% based on that of the resin layer. The preparation method of the film-coated modified propping agent is that the resin layer is coated on the outer surface of the matrix. The film-coated modified propping agent can be applied in fields of fracturing exploitation of oil and gas wells, is helpful to increase sand ratio and reduce usage amount of fracturing liquid, can effectively prevent backflow phenomenon, alleviates insertion of the propping agent, increases crack diversion capability, prolongs fracturing validity period, is helpful to increase oil output, reduces water yield and has significant meaning for solving the exploitation of low permeability oil field.
Owner:亿利沙材料科技有限责任公司

Method for preparing cold-bonded pellets from iron containing sludge by compound adhesive

InactiveCN101775489AReduce the amount of non-ferrous materialsReduce pollutionCelluloseSodium Bentonite
The invention relates to a method for preparing cold-bonded pellets from sludge containing iron by an compound adhesive, belonging to the technical field of adhesives for metallurgical ironmaking. The method of the invention comprises the following concrete steps: adopting the compound adhesive of an inorganic adhesive and an organic adhesive, wherein the organic adhesive in the compound adhesive comprises the following raw materials: vinyl acetate, acroleic acid, sodium cellulose glycolate, polyvinyl alcohol, polyisobutylene, molasses and coal tar; and the inorganic adhesive comprises the following raw materials: bentonite, calcium oxide, basic sodium silicate, sodium chloride, talcum powder and light calcium carbonate. When the organic adhesive and the inorganic adhesive in the adhesive are prepared, the components are proportioned and controlled strictly in a proper order, so that the defects of one adhesive singly used can be avoided, and the compound adhesive has good caking property on the iron containing sludge. The method of the invention recycles iron from iron containing sludge and changes waste into resources, thereby reducing pollution of storage and transport on the environment, and saving the energy consumption in the sintering and high furnace production.
Owner:TONGJI UNIV

Raw material mixing ratio and preparation method of red mud ceramsite

The invention discloses a raw material mixing ratio and preparation method of red mud ceramsite. The red mud ceramsite is prepared from the following raw materials by weight percent: 15 to 75 percentof red mud, 10 to 65 percent of building waste or sludge or bauxite or coal ash or coal gangue or clay or binder, 1 to 20 percent of water, 5 to 35 percent of crushed glass or SiO2, 5 to 25 percent ofcement and 10 to 45 percent of foaming agent or gas forming agent or expansion agent or other additives (comprising bentonite, NaNO3 powder, starch and metal powder such as aluminum, zinc, calcium carbide, magnesium and the like). The binder, the gas forming agent and the foaming agent comprise all types available in the market at present. The production process comprises the steps of treating raw materials, pelletizing, granulating, layering screening, baking by a temperature box, calcining raw ceramsite, and cooling. The ceramsite prepared in the invention meets the national and relevant industrial safety requirements and indexes and has excellent acoustic performance and is high in high temperature resistance, high pressure resistance and strength. In addition, a great amount of solidwaste is adopted, so that the environmental protection significance is outstanding. Production equipment utilizes bio-fuel, thereby saving the energy compared with a conventional calcining productionmethod.
Owner:GUILIN UNIVERSITY OF TECHNOLOGY

Linseed oil microcapsules capable of quickly forming films to timely repair scratches and preparation method thereof

The invention relates to linseed oil microcapsules capable of quickly forming films to timely repair scratches and a preparation method thereof. According to the microcapsules, linseed oil is used as capsule cores, gelatin is used as a wall material, the capsules are spherical, the average capsule diameter is 20 microns, the capsule walls are uniform, and the surfaces of the microcapsules are smooth. The preparation method comprises the steps of preparing gelatin emulsion and linseed oil emulsion respectively, dripping the linseed oil emulsion into the gelatin emulsion while stirring, and emulsifying the two phases together; adding glacial acetic acid to adjust the pH value of the solution to 4.8, adding an aqueous solution of anhydrous sodium sulfate, and cooling to 20 DEG C to wrap the capsule walls compactly; dripping formaldehyde while stirring, curing capsule films to obtain a solution, and performing freeze drying on the solution to obtain white linseed oil microcapsule solid powder. The gelatin and the linseed oil are emulsified respectively and then emulsified together, so that the linseed oil microcapsules are good in shape, easy in capsule diameter control and stable in solvents such as water, dimethyl benzene and the like; after the microcapsules are added into a coating, the light scattering is weak, and the appearance of the coating is not affected; the linseed oil flowing out after the microcapsules are broken can quickly form the films in oxygen to timely repair the scratches.
Owner:SOUTH CENTRAL UNIVERSITY FOR NATIONALITIES +2

Ultralow-density ceramsite proppant prepared from silica and preparation method of ceramsite proppant

The invention relates to an ultralow-density ceramsite proppant prepared from silica and a preparation method of the ceramsite proppant. The ceramsite proppant consists of the following raw materials in parts by weight: 60-80 parts of silica, 5-30 parts of low-aluminum and high-iron bauxite, 1-7 parts of limestone, 1-6 parts of talcum and 1-7 parts of forsterite powder. The preparation method comprises the following steps: breaking and intermediately crushing the raw materials, proportioning the raw materials in proportion, grinding the raw materials by virtue of a wet-process ball mill, removing large particles by virtue of a sieve of 80-110 mesh, and spray-drying so as to obtain a powdery material; forcedly balling the powdery material, drying the material until water content is less than 5wt%, and sieving by virtue of 18-30 mesh so as to obtain a half-finished product; and calcining the half-finished product to obtain a product, cooling the product to room temperature and sieving the product by virtue of 20-40 mesh so as to obtain a finished product with proper grain size, wherein the grain size of the broken raw materials is less than 0.056mm. The ceramsite proppant disclosed by the invention is low in apparent density, high in strength, low in turbidity, relatively low in acid solubility, and the ceramsite proppant is excellent in roundness and sphericity; and the preparation method is simple and is easy to operate.
Owner:ZIBO JIAFENG MINING

Tectorial membrane proppant as well as preparation method and application thereof

The invention discloses a tectorial membrane proppant as well as a preparation method and the application thereof. The tectorial membrane proppant is characterized by consisting of the following components in part by weight: 150 to 250 parts of Kubuqi desert sand, 2 to 20 parts of resin binder and curing agent and 5 to 50 parts of water, wherein the using amount of the curing agent is 10 to 50 percent of the weight of the resin binder and the curing agent; the resin is waterborne epoxy bisphenol A resin; and the curing agent is waterborne epoxy fatty amine curing agent. The tectorial membrane proppant is prepared by stirring the components uniformly, completely curing, dispersing uniformly and sieving. The tectorial membrane proppant is applied to the field of fracturing exploitation of petroleum and natural gas oil. The invention has the characteristics that the production process is simple; the product has low relative density, high strength, low breakage rate and high roundness, sphericity and chemical inertness; and pollution in the preparation process is avoided. The invention is widely applied to fracturing of oil field and gas field, so that the using amount of fracturing liquid is reduced, the flow guide ability of crack is improved, the fracturing useful life is prolonged, the oil yield is facilitated, and important significance of solving problem about exploitation of low-permeability oil field is achieved.
Owner:亿利沙材料科技有限责任公司

Process and device for preparing nano-powder by utilizing ultrasonic static electricity

The invention provides a process and a device for preparing nano-powder by utilizing ultrasonic static electricity. The process and the device combine the advantages of ultrasonic atomization and static atomization and skillfully overcome the disadvantages of the two. The process mainly comprises the following steps that: raw material is heated to be in a liquid state through a heating furnace, degassed through a degassing device and then conveyed to an atomizer through a pipeline; the raw material in the atomizer is first precharged via a precharging device and then is guided into a nozzle of a piezoelectric-type ultrasonic atomization system through a flow-guiding pipe in order to be atomized; the obtained material is accelerated through a primary acceleration-ring group, enters an inductive charging ring, and is charged and atomized again; the atomized raw material is accelerated through a secondary acceleration-ring group, joined and mixed through a Y-shaped pipe; mixed compounded fog drops are irradiated with an alpha ray source to remove surface charge; the charge-removed fog drops pass through a flow-guiding device (a resistance-wire heating pipe is arranged in the flow-guiding device to perform corresponding thermal decomposition on the fog drops needing thermal decomposition), enter a condenser, are condensed into solid powder; and the solid power leaves the atomizer and then enters a collection device in order to be collected. Therefore, the nano-powder with product stability, high performance, narrow particle distribution, uniform particle distribution, good monodispersity, little agglomeration, high purity and good sphericity can be prepared by utilizing equipment which is simple, low in cost, free from pollution, easy to control and suitable for large-scale continuous industrial production.
Owner:李洋

A film-coated modified proppant and its preparation method and application

The invention discloses a film-coated modified propping agent, and a preparation method and an application thereof. The film-coated modified propping agent is composed of a matrix and a resin layer uniformly coated out of the matrix, wherein the matrix is Hobq quartz sand; the resin layer is 1-10 wt% based on that of the matrix; and the resin layer comprises a resin binder and a curing agent, wherein the resin binder is bisphenol A epoxy resin, polyurethane resin or a combination thereof, the curing agent is an aliphatic polyamine curing agent an oralicyclic amine curing agent, and the usage amount of the curing agent is 10-50 wt% based on that of the resin layer. The preparation method of the film-coated modified propping agent is that the resin layer is coated on the outer surface of the matrix. The film-coated modified propping agent can be applied in fields of fracturing exploitation of oil and gas wells, is helpful to increase sand ratio and reduce usage amount of fracturing liquid, can effectively prevent backflow phenomenon, alleviates insertion of the propping agent, increases crack diversion capability, prolongs fracturing validity period, is helpful to increase oil output, reduces water yield and has significant meaning for solving the exploitation of low permeability oil field.
Owner:亿利沙材料科技有限责任公司

Cultivation method of novel germplasm of colorized brassica oleracea L.var.capitata

The invention belongs to the technical field of genetic breeding of plants, and specifically relates to a cultivation method of a novel germplasm of colorized brassica oleracea L.var.capitata. The cultivation method is characterized in that parents of the cultivation method comprise brassica oleracea L.var.capitata and ornamental kale; the male parent is the brassica oleracea L.var.capitata, and the female parent is the ornamental kale; or, the female parent is the brassica oleracea L.var.capitata, and the male parent is the ornamental kale; the ornamental kale is b.oleracea L.var.acephala DC.; and more preferably, the genotype of the male parent is GGSSHH, and the genotype of the female parent is RRCChh; or, the genotype of the male parent is RRSShh, and the genotype of the female parentis GGSSHH. According to the invention, when the breeding germplasm is selected, the b.oleracea L.var.acephala DC. with strong ornamental property and cold-resistant property is selected, and the brassica oleracea L.var.capitata with sweet and soft mouth feel, and good balling property and ball shape and suitable for uncooked eating is selected as a parent material, so that the cultivated colorizedbrassica oleracea L.var.capitata has the characteristics that the color variety is rich; the color is bright; the ornamental property is strong; the cold-resistant property is strong; the eating quality is good; the mouth feel is sweet and crisp; the colorized brassica oleracea L.var.capitata is suitable for uncooked eating; and the balling property is relatively good.
Owner:BEIJING ACADEMY OF AGRICULTURE & FORESTRY SCIENCES +1

Sulfhydrylation calcium alginate microspheres as intestinal drug delivery carrier and preparation method of sulfhydrylation calcium alginate microsphere

The invention relates to sulfhydrylation calcium alginate microspheres as an intestinal drug delivery carrier and a preparation method of the sulfhydrylation calcium alginate microsphere. The method comprises the following steps: mixing sodium alginate with sulfhydrylation calcium alginate according to the mass ratio of (1 to 8) to 1 and preparing a solution with the mass concentration of 0.5 to 5percent, then adding an oil phase containing a surfactant and emulsifying at room temperature at 200 to 900 rpm for 45 minutes, adding CaCl2 powder and continuously stirring at 100 to 400 rpm for 0.5to 3 hours to realize cross-linking and solidifying of the microspheres, carrying out centrifugal demulsification, washing and then screening the microspheres to obtain the sulfhydrylation calcium alginate microspheres. The sulfhydrylation calcium alginate microspheres prepared with an emulsification method disclosed by the invention have uniform and controllable particle size and good monodispersity. The prepared sulfhydrylation calcium alginate microspheres have strong mucosal adhesion properties in small intestine and can prolong the residence time of the microspheres in the intestine, sothat the long-acting administration effect is achieved. Therefore, the sulfhydrylation calcium alginate microspheres prepared with the preparation method disclosed by the invention have potential market application prospects in the fields of a drug delivery system for bioactive drugs such as protein, polypeptide and the like as well as intestinal targeted drug delivery.
Owner:SICHUAN UNIV

Mesoporous silica nanosphere with ultrahigh specific surface area and preparation method thereof

The invention relates to a mesoporous silica nanosphere with an ultrahigh specific surface area and a preparation method of the mesoporous silica nanosphere. The preparation method of the mesoporous silica nanospheres with the ultrahigh specific surface area comprises the following steps: (1) dissolving tetraethoxysilane in an ethanol solution, and magnetically stirring and uniformly mixing to obtain a precursor solution A; and uniformly mixing ammonia water, water and a pore-forming agent to obtain a precursor solution B; (2) equivalently sucking the precursor solution A and the precursor solution B, placing the precursor solution A and the precursor solution B on a micro-injection pump, and quickly mixing the precursor solution A and the precursor solution B through a micro-channel reactor at the same injection speed to obtain a micro-emulsion; and (3) standing the micro-emulsion, carrying out water bath heating demulsification, carrying out suction filtration, drying, and carrying out high temperature calcination to obtain the mesoporous silica nanospheres. According to the preparation method disclosed by the invention, the mesoporous silica nanospheres with the specific surfacearea of about 700-1860m < 2 > / g can be rapidly and continuously prepared, the pelletizing effect is good, and the process time is short.
Owner:SHIHEZI UNIVERSITY

Preparation method of manganese doped double-shell-layer calcium carbonate hollow microsphere CO2 adsorbent

The invention discloses a preparation method of a manganese doped double-shell-layer calcium carbonate hollow microsphere CO2 adsorbent. The preparation method comprises following steps: cane sugar solution hydro-thermal reaction is carried out to prepare carbon spheres; the carbon spheres are taken as a sacrificial template, and are added into a mixed solution of a calcium salt and a manganese salt, and then water bath processing, drying, and roasting are carried out so as to obtain the manganese doped double-shell-layer calcium carbonate hollow microsphere CO2 adsorbent. According to the preparation method, the calcium/manganese ratio, the carbon sphere template, and solvent composition are adjusted, so that accurate control on the shell layer thickness, microsphere size, and the calcium/manganese ratio in the manganese doped double-shell-layer calcium carbonate hollow microsphere can be realized, the prepared manganese doped double-shell-layer calcium carbonate hollow microsphere CO2 adsorbent is relatively high in adsorption capacity and stability in adsorption and desorption circulation; the highest initial adsorption capacity of the adsorbent with the best performance is 0.62g CO2/g adsorbent, and the adsorption capacity is still maintained to be 0.53g CO2/g adsorbent after 25 times of circulation.
Owner:TIANJIN UNIV
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