Multi-parameter water quality detection method and multi-parameter water quality detector based on same

A detection method and multi-parameter technology, applied in the preparation of test samples, color/spectral property measurement, etc., can solve the problems of inability to meet multi-parameter online real-time detection, high risk of secondary pollution, single detection index, etc. The equipment is convenient to use, the measurement time is short, and the effect of improving the detection accuracy

Inactive Publication Date: 2016-07-27
QINGDAO JIAMING MEASUREMENT & CONTROL TECH
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Problems solved by technology

The indicators that need to be tested for comprehensive evaluation of water quality indicators include chemical oxygen demand, ammonia nitrogen, permanganate index, total nitrogen, and total phosphorus. ), nitrite nitrogen (HJ/T197-2005), nitrate nitrogen (HJ/T198-2005), total nitrogen (HJ/T199-2005), sulfide (HJ/T200-2005) meet the Ministry of Environmental Protection standards For the measurement items of the method, according to the national standard, the detection methods and reagents used for each parameter are different, such

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  • Multi-parameter water quality detection method and multi-parameter water quality detector based on same
  • Multi-parameter water quality detection method and multi-parameter water quality detector based on same
  • Multi-parameter water quality detection method and multi-parameter water quality detector based on same

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specific Embodiment approach

[0026] Prepare nitrate nitrogen standard stock solution and nitrite nitrogen standard stock solution:

[0027] Preparation of nitrate nitrogen standard stock solution (1000mg / L): Weigh 3.034g of high-grade pure sodium nitrate (NaNO3) dried at 105°C to 110°C for 2 hours, dissolve in water, transfer to a 500mL volumetric flask, add water to dilute to the marked line , shake well.

[0028] Preparation of nitrite nitrogen standard stock solution (1000mg / L): Weigh 2.463g of high-grade pure sodium nitrite (NaNO2) dried at 105°C to 110°C for 2 hours, dissolve in water, transfer to a 500mL volumetric flask, and dilute with water to the mark and shake well.

[0029] Prepare standard solutions from stock solutions:

[0030] Utilize nitrate nitrogen standard stock solution to make the nitrate standard solution that nitrate nitrogen content is 0,0.2,0.5,1.0,1.5,2.0mg / L, utilize nitrite nitrogen standard stock solution to make nitrite nitrogen content be 0, 0.05, 0.10, 0.20, 0.40, 0.50m...

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Abstract

A multi-parameter water quality detection method comprises the steps as follows: (1) preparing a standard solution, (2) creating a standard curve, 3) sampling a sample, 4) preprocessing the sample, 5) performing experimental determination and 6) calculating permanganate index concentration, ammonia nitrogen concentration and total nitrogen concentration. A multi-parameter water quality detector comprises a main unit body provided with a storage bin and an experiment bin. According to the detection method, detection of a permanganate index, ammonia nitrogen, total nitrogen, nitrite nitrogen and nitrate nitrogen of a to-be-detected substance is realized through an absorption spectrum, the operation procedure is simplified, the on-line condition of the detector is facilitated, the defects of many required instruments and high cost of the different traditional methods are overcome, multiple parameters can be detected on line in real time by one detector, the measurement time is short, the accuracy is high, the detection limit is low, the lowest detection limit of total nitrogen is 0.5 mg/L, the lowest detection limit of ammonia nitrogen is 0.1 mg/L, the lowest detection limit of the permanganate index is 0.1 mg/L, and the detection requirements of the Quality standard for ground water and the Environmental quality standards for surface water (GB3838-2002) for total nitrogen, ammonia nitrogen and the permanganate index can be met.

Description

technical field [0001] The invention belongs to the field of water quality detection, and relates to an experimental method and a monitor for on-line detection of multi-parameters of water quality realized by gas-phase molecular absorption spectroscopy. Background technique [0002] At present, the country attaches great importance to water quality monitoring. There are many instruments and methods that can be used for water quality testing. Gas-phase molecular absorption spectrometer is one of them. It can be widely used in drinking water production, environmental monitoring, petrochemical industry, sanitation and epidemic prevention, food industry, soil, etc. Water quality analysis in various fields such as chemical fertilizers, chemical reagents, papermaking, leather, printing and dyeing, industrial and mining enterprises, civil engineering, marine and fishery, and hydrological monitoring. The indicators that need to be tested for comprehensive evaluation of water quality...

Claims

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Application Information

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IPC IPC(8): G01N21/31G01N1/28
CPCG01N21/31G01N1/28
Inventor 吴得福高心岗李霞王强李洪杰秦杰朱保超梁荣林隋宗斌孟璐
Owner QINGDAO JIAMING MEASUREMENT & CONTROL TECH
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