A clean and efficient production process of diosgenin

A technology of diosgenin and production process, applied in the directions of microorganisms, food processing, additional food elements, etc., can solve problems such as difficulty in drinking water for humans and animals, destruction of forests, soil acidification, etc., and achieve the effects of reducing encapsulation and improving extraction efficiency.

Active Publication Date: 2017-12-05
十堰赟天生物科技发展有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The environmental pollution problem caused by extracting diosgenin from turmeric has always been the bottleneck of the industry
About 500 tons of strong acid wastewater will be produced for every ton of saponin produced. The COD concentration in the wastewater is about 32,000 mg / liter, and its pollution level is 12 times higher than that of papermaking wastewater. After treatment, the COD content in the wastewater can be reduced to 500 to 800 mg / L or so, but this is still far below the COD content of 100 mg / L stipulated in the first-level standard for the comprehensive discharge of corporate sewage
Perennial sewage can lead to difficulty in drinking water for humans and animals, reduce crop production, and destroy forests and vegetation, lead to soil acidification, affect groundwater, and pollute water sources.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] A clean and efficient production process of diosgenin, comprising the following steps:

[0030] The first step: first wash the fresh turmeric from the sediment, drain the water, and then beat it together with 95v / v% ethanol. The slurry is heated and extracted in a high-pressure tank at 2-5 atmospheres and 60-95°C for 1-5 hours. Then filter, the filtrate is concentrated and recovered, the concentrated filtrate is dried and pulverized to obtain the extract powder, which is diosgenin coarse powder; wherein the weight-to-volume ratio of fresh turmeric and 95v / v% ethanol is 1g: (1-5)ml .

[0031] The second step: the coarse powder of diosgenin is mixed with the acid aqueous solution in the acid hydrolysis tank for acid hydrolysis, the acid of the acid aqueous solution can be sulfuric acid or sulfurous acid or hydrochloric acid or nitric acid or nitrous acid or formic acid, etc., the amount of the acid aqueous solution is covered by the liquid surface The coarse diosgenin powd...

Embodiment 2

[0037] A clean and efficient production process of diosgenin, comprising the following steps:

[0038] The first step: first wash the fresh turmeric from the sediment, drain the water, and then make a pulp with water-saturated n-butanol. The slurry is heated and extracted in a high-pressure tank at 2-5 atmospheres and 60-95°C for 1-5 hours. Then filter, the filtrate is concentrated and recovered, the concentrated filtrate is dried and pulverized to obtain extract powder, which is diosgenin coarse powder; wherein the weight-to-volume ratio of fresh turmeric to water-saturated n-butanol is 1g: (1-5)ml.

[0039] Step 2: Dioscin coarse powder is mixed with acid aqueous solution in acid hydrolysis tank for acid hydrolysis. The acid of acid aqueous solution is sulfuric acid or sulfurous acid or hydrochloric acid or nitric acid or nitrous acid or formic acid, etc. The amount of acid aqueous solution is to cover dioscin on the liquid surface The coarse powder shall prevail, acid water...

Embodiment 3

[0045] A clean and efficient production process of diosgenin, comprising the following steps:

[0046] The first step: first wash the fresh turmeric from the sediment, drain the water, and then make a pulp with water-saturated n-butanol. The slurry is heated and extracted in a high-pressure tank at 2-5 atmospheres and 60-95°C for 1-5 hours. Then filter, the filtrate is concentrated and recovered, and the filtrate concentrated 5-10 times is used as dioscin crude saponin slurry.

[0047] The second step: the dioscin crude saponin slurry is mixed with the acid aqueous solution in the acid hydrolysis tank for acid hydrolysis, the acid in the acid aqueous solution is sulfuric acid or sulfurous acid or hydrochloric acid or nitric acid or nitrous acid or formic acid, etc., and the acid aqueous solution is mixed with the dioscin crude saponin slurry A reaction liquid is formed, and the pH value of the reaction liquid in the acidolysis tank is 1-2; the acidolysis temperature is 95° C.,...

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PUM

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Abstract

The invention provides a clean and efficient diosgenin production technology .The production technology comprises the steps of extracting dioscin coarse powder from fresh yellow ginger, conducting acidolysis on the dioscin coarse powder, then adding 1-50 times, by weight, of carbonate, a mixture of carbonate and silica gel powder, or a mixture of carbonate and perlite fine powder for sufficient mixing to obtain a dry muddy mixture, conducting drying and smashing to obtain mixture fine powder, and extracting the mixture fine powder with 120# gasoline or petroleum ether to obtain diosgenin .Powder obtained after diosgenin extraction serves as boiler fuel to be burnt .Residues obtained after diosgenin extraction are rich in starch and can be used for selenium-enriched fermentation to produce ethyl alcohol, and residues obtained after ethyl alcohol production through selenium-enriched fermentation can be used for making fertilizer or feed special for yellow ginger .Residues obtained after alcoholic fermentation are further dried to make selenium-enriched feed or selenium-enriched fertilizer .During diosgenin production, acid neutralization or washing is not needed, and acid water discharging is completely avoided.

Description

technical field [0001] The invention belongs to the field of biochemical industry and relates to a clean and efficient production process of diosgenin, in particular to a highly efficient and pollution-free production method of diosgenin. Background technique [0002] Diosgenin is an important pharmaceutical raw material. More than two hundred kinds of drugs can be synthesized by using diosgenin, which has a wide range of uses. Diosgenin is mainly present in the rhizomes of Dioscorea plants in the form of diosgenin. Dioscorea scutellaria is mainly cultivated in my country, and the rhizome of Dioscorea scutellaria is harvested to prepare diosgenin. The key technology for preparing diosgenin from the rhizome of Dioscorea shield leaf is to adopt a suitable method to break the glycosidic bond of diosgenin and desugar to obtain diosgenin. [0003] At present, the preparation methods of diosgenin mainly include acid hydrolysis, biological hydrolysis (enzymatic hydrolysis) and r...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07J71/00C12P7/08A23K10/37A23K20/20C05G1/00C12R1/865
CPCC05D9/02C07J71/0005C12P7/08C05F5/008Y02P60/87
Inventor 董静洲艾训儒姚兰雷灿
Owner 十堰赟天生物科技发展有限公司
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