A clean and efficient production process of diosgenin
A technology of diosgenin and production process, applied in the directions of microorganisms, food processing, additional food elements, etc., can solve problems such as difficulty in drinking water for humans and animals, destruction of forests, soil acidification, etc., and achieve the effects of reducing encapsulation and improving extraction efficiency.
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Embodiment 1
[0029] A clean and efficient production process of diosgenin, comprising the following steps:
[0030] The first step: first wash the fresh turmeric from the sediment, drain the water, and then beat it together with 95v / v% ethanol. The slurry is heated and extracted in a high-pressure tank at 2-5 atmospheres and 60-95°C for 1-5 hours. Then filter, the filtrate is concentrated and recovered, the concentrated filtrate is dried and pulverized to obtain the extract powder, which is diosgenin coarse powder; wherein the weight-to-volume ratio of fresh turmeric and 95v / v% ethanol is 1g: (1-5)ml .
[0031] The second step: the coarse powder of diosgenin is mixed with the acid aqueous solution in the acid hydrolysis tank for acid hydrolysis, the acid of the acid aqueous solution can be sulfuric acid or sulfurous acid or hydrochloric acid or nitric acid or nitrous acid or formic acid, etc., the amount of the acid aqueous solution is covered by the liquid surface The coarse diosgenin powd...
Embodiment 2
[0037] A clean and efficient production process of diosgenin, comprising the following steps:
[0038] The first step: first wash the fresh turmeric from the sediment, drain the water, and then make a pulp with water-saturated n-butanol. The slurry is heated and extracted in a high-pressure tank at 2-5 atmospheres and 60-95°C for 1-5 hours. Then filter, the filtrate is concentrated and recovered, the concentrated filtrate is dried and pulverized to obtain extract powder, which is diosgenin coarse powder; wherein the weight-to-volume ratio of fresh turmeric to water-saturated n-butanol is 1g: (1-5)ml.
[0039] Step 2: Dioscin coarse powder is mixed with acid aqueous solution in acid hydrolysis tank for acid hydrolysis. The acid of acid aqueous solution is sulfuric acid or sulfurous acid or hydrochloric acid or nitric acid or nitrous acid or formic acid, etc. The amount of acid aqueous solution is to cover dioscin on the liquid surface The coarse powder shall prevail, acid water...
Embodiment 3
[0045] A clean and efficient production process of diosgenin, comprising the following steps:
[0046] The first step: first wash the fresh turmeric from the sediment, drain the water, and then make a pulp with water-saturated n-butanol. The slurry is heated and extracted in a high-pressure tank at 2-5 atmospheres and 60-95°C for 1-5 hours. Then filter, the filtrate is concentrated and recovered, and the filtrate concentrated 5-10 times is used as dioscin crude saponin slurry.
[0047] The second step: the dioscin crude saponin slurry is mixed with the acid aqueous solution in the acid hydrolysis tank for acid hydrolysis, the acid in the acid aqueous solution is sulfuric acid or sulfurous acid or hydrochloric acid or nitric acid or nitrous acid or formic acid, etc., and the acid aqueous solution is mixed with the dioscin crude saponin slurry A reaction liquid is formed, and the pH value of the reaction liquid in the acidolysis tank is 1-2; the acidolysis temperature is 95° C.,...
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