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Folium Isatidis freshly-pressed lyophilized powdery decoction pieces and preparation process thereof

A technology of dry powder and preparation technology, which is applied in the field of processing technology of Chinese medicine Daqingye decoction pieces, can solve the problems of time-consuming and energy-consuming, non-polar active ingredients are difficult to extract, etc., and achieves convenience for storage and transportation, significant social significance and economic Significance, the effect of stable quality of decoction pieces

Inactive Publication Date: 2016-10-12
徐漫
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The preparation process of granular decoction pieces, the extraction is not only time-consuming and energy-consuming, but also because a large amount of water is often used as a solvent, it is difficult to extract the non-polar active ingredients in the medicinal materials
In addition, since the Folium Folium medicinal material used for extraction is also dried and stored for a long time, the loss of active ingredients is also great

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0012] The freshly collected Folium Folium medicinal materials are cleaned, washed with water to remove the sediment, and squeezed with a press to extract the juice while it is fresh. Add 3 times the amount of tap water to the obtained dregs, stir for 20 minutes, and press with a plate-and-frame filter press to extract the juice. The remaining medicinal dregs are squeezed with a press to extract the juice. The above-mentioned 3 concoctions were combined and filtered with a 100-mesh sieve. The filtrate was concentrated under reduced pressure and the temperature was set at 65 °C. When the relative density of the concentrated extract was 1.15, the extract was frozen in a -80°C refrigerator for 6 hours. Take out the east knot, freeze-dry, the pressure is 0.09Mpa, the temperature is -20 ℃, dry for 24 hours. Take out the freeze-dried product, crush it at low temperature, pass through an 80-mesh sieve, the moisture content is not higher than 12%, pack it into a bag, 1kg / bag, add t...

Embodiment 2

[0014] The freshly collected Folium Folium medicinal materials are cleaned, washed with water to remove the sediment, and squeezed with a press to extract the juice while it is fresh. Add 5 times the amount of tap water to the obtained dregs, stir for 30 minutes, and press with a plate-and-frame filter press to extract the juice. The remaining medicinal dregs are squeezed with a press to extract the juice. The above-mentioned 3 concoctions were combined and filtered with an 80-mesh sieve. The filtrate was concentrated under reduced pressure and the temperature was set at 70 °C. When the relative density of the concentrated extract was 1.10, the extract was frozen in a -80°C refrigerator for 8 hours. Take out the east knot, freeze-dry, the pressure is 0.08Mpa, the temperature is -40 ℃, dry for 48 hours. Take out the freeze-dried product, crush it at low temperature, pass through a 60-mesh sieve, the moisture content is not higher than 12%, bag it, 1kg / bag, add the bagged ant...

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PUM

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Abstract

The invention discloses a freshly squeezed freeze-dried powdered decoction piece of Folium Folium and a preparation process thereof. In this process, after the Folium Folium medicinal material is harvested, it is cleaned, rinsed, squeezed while it is fresh, and the medicinal juice is filtered. The dregs are mixed with water, filtered and pressed. The obtained medicinal juices are combined, concentrated under reduced pressure, freeze-dried, and the freeze-dried product is collected, pulverized and packed in vacuum. The Folium Folium powder decoction pieces prepared by this method retain the polar and non-polar active ingredients in the medicinal material at the same time to the greatest extent. The decoction pieces are convenient for storage and transportation, convenient for dispensing, controllable in quality, and reliable in curative effect, which is of great significance to guarantee the clinical curative effect of traditional Chinese medicine. The popularization and implementation of this Law will have significant social and economic benefits.

Description

technical field [0001] The invention belongs to the field of processing traditional Chinese medicinal materials, and in particular relates to a processing technology for decoction pieces of the traditional Chinese medicinal Folium Folium. Background technique [0002] The traditional Chinese medicine Daqingye is the cruciferous plant Isatis indigo Isatis indigotica Dry leaves of Fort. Harvest in 2~3 times in summer and autumn, remove impurities and dry in the sun. This product has the effects of clearing away heat and detoxifying, cooling blood and eliminating spots. It is mainly used for the treatment of febrile diseases with high fever and polydipsia, coma, rash, vomiting blood, epistaxis, dysentery, erysipelas, aphtha, mumps, and sore throat. [0003] The commonly used processing methods of Folium Folium decoction pieces are: harvest in summer and autumn, remove impurities, dry in the sun, and pack for storage and transportation. Such herbal decoction pieces are bulky,...

Claims

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Application Information

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IPC IPC(8): A61K36/315A61K9/14
CPCA61K36/315A61K9/14A61K2236/31A61K2236/331A61K2236/51
Inventor 徐漫
Owner 徐漫