3D printed food package ink and preparation method thereof
A food packaging and 3D printing technology, applied in the field of 3D printing materials, can solve the problems of poor food packaging barrier effect and environmental pollution, and achieve the effect of small porosity, small printing error and high resolution
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Embodiment 1
[0020] The gypsum raw material is crushed and homogenized in three stages to obtain gypsum blocks with a particle size of 10 cm, heated to 55°C in the reactor, drained of condensed water, and then injected with 1.5 MPa saturated steam, dried for 6 hours, and then drained of excess steam; Dry for 3 hours, pressure 0.5MPa, temperature 150°C, dry for 8 hours, and grind the dried material to get gypsum powder;
[0021] Add 10.0g of DETA and 155.0g of nano-silicon carbide into the grinder, and grind for 12 hours at a speed of 500r / min;
[0022] Add 50.0g of absolute ethanol to the mixer, the mixture of ground nano-silicon carbide and DETA, 180.0g of epoxy resin, mix well, keep warm at 50°C for 6h, add 600.0g of gypsum powder and 5.0g of ultramarine blue pigment according to the formula , and mix evenly to obtain 1000g of base ink.
[0023] Add 25g of citric acid and 100g of epoxy resin to 875g of base ink, and mix evenly to prepare 1000g of 3D printing food packaging ink.
[0024...
Embodiment 2
[0026] The gypsum raw material is crushed in three stages and homogenized to obtain gypsum blocks with a particle size of 20cm, which are heated to 60°C in the reactor, and the condensed water generated is removed, then 3.5MPa saturated steam is introduced, dried for 5 hours, and then the excess steam is drained; Dry for 2 hours, pressure 0.3MPa, temperature 160°C, dry for 7 hours, and grind the dried material to get gypsum powder;
[0027] Add 200.0g of DETA and 20.0g of nano-silicon carbide into the grinder, and grind for 4 hours at a speed of 2000r / min;
[0028] Add 5.0g of absolute ethanol to the mixer, the mixture of ground nano-silicon carbide and DETA, 40.0g of epoxy resin, mix evenly, keep warm at 55°C for 4.5h, add 732.0g of gypsum powder according to the formula, and 3.0 of peacock blue pigment g, mix evenly to obtain 1000g of base ink.
[0029] Add 5g of citric acid and 100g of epoxy resin to 895g of base ink, and mix evenly to prepare 1000g of 3D printing food pac...
Embodiment 3
[0032] The gypsum raw material is crushed in three stages and homogenized to obtain gypsum blocks with a particle size of 15cm, heated to 57°C in the reactor, draining the condensed water, and then injecting 2.5MPa saturated steam, drying for 5.5h, and then draining the excess steam ;Dry for 2.5 hours, pressure 0.4MPa, temperature 155°C, dry for 7.5 hours, and grind the dried material to get gypsum powder;
[0033] Add 5.0g of DETA and 20.0g of nano-silicon carbide into the grinder, and grind for 8 hours at a speed of 1000r / min;
[0034] Add 5.0g of absolute ethanol to the mixer, the mixture of ground nano-silicon carbide and DETA, 40.0g of epoxy resin, and mix evenly. After 5 hours at 56°C, add 927.5g of gypsum powder and 2.5g of azo red pigment according to the formula. g, mix evenly to obtain 1000g of base ink.
[0035] Add 25g of sodium citrate to 975g of base ink and mix evenly to obtain 1000g of 3D printing food packaging ink.
[0036] Add 520g of 3D printing food pack...
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