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A technology of protein expression and detection method, which is applied in the field of detection of protein expression in live motor neurons, and can solve problems such as obstacles to the establishment of fundamental treatments for SMA
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Embodiment 1
[0094] Example 1: Detection of SMN Protein Expression Using Lymphoblasts
[0095] (1) Lymphoblastization treatment
[0096] Blood samples obtained from normal persons were sampled in heparin tubes, superimposed on Ficoll solution, centrifuged at 2000 rpm for 15 minutes, and peripheral blood mononuclear cells were separated and sampled. Next, lymphoblasticization was performed by using the transformation method with Epstein-Barr virus.
[0097] Blood samples obtained from type I SMA patients were also treated in the same manner as blood samples obtained from normal individuals.
[0098] (2) Determination of SMN protein expression
[0099] In a centrifuge tube, the normal human-derived peripheral blood mononuclear cell lymphoblasts obtained in the above (1) were sampled, and the cells were fixed with 4% p-formaldehyde-phosphate buffer. Next, the cells were washed with a phosphate buffer solution, centrifuged at 500×g for 5 minutes, and the supernatant was removed. As a cell ...
Embodiment 2
[0116] Embodiment 2: Use the detection of the SMN protein expression that has hemolysis method
[0117] (1) Hemolysis treatment
[0118] Blood was collected from a normal person, and 2 mL of blood was sampled in a heparin tube and mixed by inversion. Next, take 0.5 mL of blood in a centrifuge tube as a hemolysis / fixation solution, and add BD Phosflow TM Lyse / Fix Buffer (BD Biosciences), after standing at 37°C for 10 minutes, centrifuge at 2300rpm for 8 minutes, remove the supernatant, wash the cells with phosphate buffer, and obtain a sample containing nucleated cells derived from blood .
[0119] Carriers and type I SMA patients were also prepared samples containing nucleated cells derived from blood by the hemolysis method in the same manner as normal persons.
[0120] (2) Determination of SMN protein expression
[0121] Add BD Phosflow to normal human nucleated cells obtained from the above (1) TM Perm Buffer II (BD Biosciences) was used as a cell membrane permeation...
Embodiment 3
[0129] Example 3: Detection of SMN protein expression per cluster after classification using surface antigen markers
[0130] Prepare samples according to the staining protocol below.
[0131] 1. Put 2 mL of peripheral blood obtained from a normal person into a tube, and add reagents to 2 mL of peripheral blood to make 100 μL of Hoechst 33342 (Molecular Probes) diluted to 5 μg / mL with PBS and Fc receptor blocking reagent (ClearBack, MTG -001,MBL) 80 μL.
[0132] 2. Plug the vial and rotate slowly at room temperature for 15 minutes in the dark.
[0133] 3. Put 500 μL of the thus treated peripheral blood into each of four 15 mL conical tubes.
[0134] 4. Add 5 μL of fluorochrome-labeled antibody (purchased from BioLegend, BD Biosciences, and MERCK) to each tube according to the following Table 5.
[0135] [table 5]
[0136]
[0137] Cloning of monoclonal antibodies:
[0138] CD66a / c / e(ASL-32),CD66b(G10F5),CD34(581),CD25(M-A251),CD33(WM53),
[0139] CD123(6H6),CD3(UCHT1)...
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