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Dispersible oil suspension containing penoxsulam, pyribenzoxim and cloquitocet-mexyl and preparation method thereof

A technology of saflufenacil and penoxsulam, which is applied in the field of pesticides, can solve the problems of incomplete and effective control of weeds in paddy fields, residual toxicity of current crops or subsequent crops, and different sensitivity of herbicides. Achieve the effects of improving physical and chemical stability, simple production equipment and methods, and eliminating dust pollution

Inactive Publication Date: 2017-01-25
ZHEJIANG TIANFENG BIOLOGICAL SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] At present, a single herbicide is limited by the safety selection of crop varieties. At the same time, the herbicide spectrum is not complete when used alone, and the occurrence of weeds in paddy fields cannot be completely and effectively controlled. Moreover, the weed resistance of a single herbicide is also serious.
Some herbicides are sensitive to different varieties of rice, or the field duration is too short, the dosage is too large, or the application is uneven, which may easily cause residual toxicity to the current crop or subsequent crops.

Method used

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  • Dispersible oil suspension containing penoxsulam, pyribenzoxim and cloquitocet-mexyl and preparation method thereof
  • Dispersible oil suspension containing penoxsulam, pyribenzoxim and cloquitocet-mexyl and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] After adding 730g of methyl oleate into the shear kettle, add 100g of emulsifier alkylphenol polyoxyethylene ether, 20g of wetting agent 2-2-octyl maleate sulfonate, and 20g of dispersant sodium lignosulfonate 30g, organic bentonite 30g, butylated hydroxyanisole 12, silicone defoamer 5g and citric acid 3g, mix and stir, add penoxsulam 30g under stirring at the speed of high-speed shearing machine 1500-10000 rpm , 30 g of saflufenacil, 10 grams of saflufenacil, cut for 10 to 40 minutes, and then grind with a sand mill until the particle size D90 is less than 5 μm, that is, the light yellow containing penoxsulam and saflufenacil , Dispersible oil-suspension concentrate of clofenac-methyl.

Embodiment 2

[0024] After adding 682g of soybean oil in the shear kettle, add 50g of emulsifier sorbitan monolaurate, 60g of alkylphenol polyoxyethylene ether, and 30g of wetting agent di-sec-octyl maleate sulfonate , dispersant TERSPERSE 2020 dispersant 25g, magnesium aluminum silicate 35g, sodium benzoate 18, silicone defoamer 8g and acetic acid 10g, mix and stir, add five After 25g of oroxsulam, 45g of saflufenacil, and 12 grams of clofenac-methyl, cut for 10 to 40 minutes, and then grind with a sand mill until the particle size D90 is less than 5 μm, the light yellow penoxsulam containing , dispersible oil suspension concentrate of saflufenacil, and clofenac-methyl.

Embodiment 3

[0026]After adding rapeseed oil 617g in the shear kettle, add emulsifier alkylphenol polyoxyethylene ether 60g, alkylphenol polyoxyethylene ether sodium sulfate 50g, fatty acid polyoxyethylene ester phosphate 5g, wetting agent cisbutylate Di-sec-octyl enedioic acid sodium sulfonate 45g, dispersant sodium lignin sulfonate 35g, xanthan gum 30g, triphenyl phosphite 45g, silicone defoamer 5g and citric acid 13g, mix and stir at high speed Add 50g of penoxsulam, 30g of saflufenacil, and 15g of clofenacyl under stirring at the speed of 1500-10000 rpm of the shearing machine, cut for 10-40 minutes, and then grind to the particle size with a sand mill If the D90 is less than 5 μm, a dispersible oil suspension containing penoxsulam, saflufenacil, and gluclofenapyr-methyl is prepared.

[0027] See Table 1 for the technical indicators of the penoxsulam, saflufenacil, and clofenac-ethyl dispersible oil suspensions of the present invention.

[0028] Table 1: Technical indicators of penoxs...

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Abstract

The present invention relates to a pesticide herbicide product, in particular to a dispersible oil suspension containing penoxsulam, saflufenacil, and cloclofenac and a preparation method thereof, wherein the distribution ratio of each component is: penoxsulam Amine 2%~8%, saflufenacil 2%~8%, cloclofenac 0.5%~3%, dispersant 1%~8%, emulsifier 5%~15%, wetting agent 0.5%~5% , 0.5% to 5% thickener, 0.5% to 8% stabilizer, 0.2% to 2% defoamer, 0.1% to 2% pH regulator, and the balance is oil-based solvent. Compared with the prior art, the penoxsulam, saflufenacil, and clofenac-ethyl dispersible oil suspension concentrate of the present invention have low toxicity to humans, animals, and beneficial organisms, can reduce the toxicity of active ingredients to applicators, and reduce the The phytotoxicity of drugs on target crops improves the control effect of herbicide products on weeds and the safety of crops. It is a low-carbon, environmentally friendly, safe and efficient dosage form.

Description

technical field [0001] The invention belongs to the technical field of pesticides, and relates to a herbicide product, in particular to a dispersible oil suspension containing penoxsulam, saflufenacil and gluclofenapyr and a preparation method thereof. Background technique [0002] Penoxsulam, chemical name 2-(2,2-difluoroethoxy)-N-(5,8-dimethoxy(1,2,4)triazole-(1,5-C ) pyrimidin-2-yl)-6-trifluoromethyl-benzenesulfonamide. It is a herbicide for post-emergence paddy fields developed by Dow AgroSciences. It was officially registered with the US EPA on September 24, 2004. It was promoted and applied in the southern rice fields of the United States in 2005, and it was registered in my country in 2008. It is a conductive strong acetolactate synthase inhibitor. The drug is absorbed by the stems, leaves, buds and roots, and then transmitted to the meristematic tissue through the xylem and phloem, inhibiting plant growth, making the growing point chlorotic, and weeds for 7-15 days...

Claims

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Application Information

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IPC IPC(8): A01N43/90A01N43/42A01N43/54A01P13/00
CPCA01N43/90A01N43/42A01N43/54
Inventor 范伟赠陈丰喜徐雅飞卓家雄王国华
Owner ZHEJIANG TIANFENG BIOLOGICAL SCI
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