Composite glass fibers and preparation method thereof
A glass fiber and pretreatment technology, applied in the field of glass fiber, can solve the problems of poor wear resistance and popularization and use
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Embodiment 1
[0019] (1) Place 1 glass fiber with a volume length of 65 μm in 1.1 volume concentration of 0.05 mol / L hypochlorous acid solution, and heat it at 65°C for 20 minutes to carry out oxidation treatment;
[0020] (2) soak 1 volume of the glass fiber after oxidation treatment in 2 volumes of silane coupling agent with a temperature of 40° C. and a volume concentration of 25% for 1 hour, then filter, wash, and dry to obtain pretreated glass fibers;
[0021] (3) 2 parts by weight of pretreated glass fiber and 1 part by weight of polylactic acid were mixed and heated at 155° C. for 35 minutes to prepare composite glass fiber A1.
Embodiment 2
[0023] (1) Place 1 glass fiber with a volume length of 78 μm in a hypochlorous acid solution with a volume concentration of 0.05 mol / L, and heat at 83°C for 28 minutes to perform oxidation treatment;
[0024] (2) soak 1 volume of the glass fiber after oxidation treatment in 5 volumes of silane coupling agent with a volume concentration of 43% and a temperature of 65°C for 1.8 hours, then filter, wash, and dry to obtain pretreated glass fibers;
[0025] (3) 5 parts by weight of pretreated glass fiber and 1 part by weight of polylactic acid were mixed and heated at 170° C. for 55 minutes to prepare composite glass fiber A2.
Embodiment 3
[0027] (1) Put a glass fiber with a volume length of 72 μm in a hypochlorous acid solution with a volume concentration of 0.1mol / L, and heat it at 70°C for 25 minutes to perform oxidation treatment;
[0028] (2) soak 1 volume of the glass fiber after oxidation treatment in 3 volumes of silane coupling agent with a temperature of 55° C. and a volume concentration of 35% for 1.5 hours, then filter, wash, and dry to obtain pretreated glass fibers;
[0029] (3) Mix 2 parts by weight of pretreated glass fiber with 1 part by weight of polylactic acid and heat at 160° C. for 45 minutes to prepare composite glass fiber A3.
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