A kind of preparation method of graphene/aluminum composite material
An aluminum composite material and graphene technology, which is applied in metal material coating process, liquid chemical plating, coating, etc., can solve the problems of severe graphene agglomeration, poor material uniformity, and poor interface bonding ability
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Embodiment 1
[0058] (1) Graphene electroless nickel plating
[0059] a. Sensitization: control SnCl 2 Sensitizer (SnCl 2 Concentration of 15g / L, HCl concentration of 10mg / L) and temperature of 20°C, graphene was added in an amount of 11mg / mL and ultrasonically oscillated for 30min, filtered, and washed with deionized water until neutral.
[0060] b. Activation: control PbCl 2 Activation solution (PbCl 2 The concentration is 0.1g / L, the concentration of HCl is 10 mL / L) and the temperature is 20°C. Add the sensitized graphene in the amount of 11 mg / mL and ultrasonically vibrate for 30 minutes, filter, and wash with deionized water until neutral .
[0061] c. Electroless nickel plating: add the sensitized and activated graphene to the electroless nickel plating solution (the concentration of nickel chloride is 25g / L, the concentration of sodium hypophosphite is 30g / L, and the concentration of glycolic acid is 15g) / L), stirring, the pH value of the plating solution was adjusted to 8 with...
Embodiment 2
[0066] (1) Graphene electroless nickel plating
[0067] a. Sensitization: control SnCl 2 Sensitizer (SnCl 2 Concentration of 24g / L, HCl concentration of 19mL / L) and temperature of 23°C, graphene was added in an amount of 12mg / mL and ultrasonically oscillated for 35min, filtered, and washed with deionized water until neutral.
[0068] b. Activation: control PbCl 2 Activation solution (PbCl 2 The concentration is 0.4g / L, the concentration of HCl is 20 mL / L) and the temperature is 23°C. Add the sensitized graphene in an amount of 12mg / mL and ultrasonically vibrate for 35min, filter, and wash with deionized water until neutral .
[0069] c. Electroless nickel plating: Add the sensitized and activated graphene to the electroless nickel plating solution in an amount of 7mg / mL (the concentration of nickel chloride is 28g / L, the concentration of sodium hypophosphite is 33g / L, and the concentration of glycolic acid is 21g / L), stirring, the pH value of the plating solution was adj...
Embodiment 3
[0074] (1) Graphene electroless nickel plating
[0075] a. Sensitization: control SnCl 2 Sensitizer (SnCl 2 Concentration of 33g / L, HCl concentration of 28mL / L) and temperature of 25°C, graphene was added in an amount of 13mg / mL and ultrasonically oscillated for 40min, filtered, and washed with deionized water until neutral.
[0076] b. Activation: control PbCl 2 Activation solution (PbCl 2 The concentration is 0.7g / L, the concentration of HCl is 30mL / L) and the temperature is 25°C. The sensitized graphene is added in an amount of 13mg / mL and ultrasonically oscillated for 40min, filtered, and washed with deionized water until neutral.
[0077] c. Electroless nickel plating: add the sensitized and activated graphene to the electroless nickel plating solution (the concentration of nickel chloride is 30g / L, the concentration of sodium hypophosphite is 35g / L, and the concentration of glycolic acid is 27g) / L), stirring, the pH value of the plating solution was adjusted to 9 wi...
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