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Method for improving detection efficiency and representativeness of chemical components of crude tobacco package

A technology of detection efficiency and chemical composition, applied in the direction of material analysis, measuring devices, scientific instruments, etc. through optical means, can solve the problems of non-representation, heavy processing workload, large differences, etc., and improve the reliability expression , increase utilization, and improve efficiency

Active Publication Date: 2017-04-26
YUNNAN KUNMING SHIPBUILDING DESIGN & RESEARCH INSTITUTE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Before the samples are tested by these two instruments, the samples need to be pretreated by tobacco leaves, and the samples need to be processed by removing stems from tobacco leaves, coarse powder, drying and refined powder. Therefore, the processing workload is large and time-consuming. However, the chemical composition detection time of the flow injection analyzer takes about 3 to 4 hours, which takes a long time and seriously affects the amount of tobacco leaf sampling.
The efficiency of testing the chemical composition of raw cigarette packs is low, which directly affects the judgment and grasp of the quality of raw tobacco purchased and stored by enterprises
Moreover, tobacco companies always use the single-point sampling value of the sample taken as the chemical composition value of the whole box of cigarettes for the detection value of the chemical composition of the original cigarette pack, which is not representative and has a large difference;
[0003] Raw tobacco leaves are agricultural products, and the chemical composition values ​​of different leaves, and even different parts of the same tobacco leaf, are very different. Therefore, sampling and inspection of a single point in the same cigarette pack cannot represent the chemical composition of the whole pack of tobacco leaves.
However, due to the time-consuming and labor-intensive inspection methods for the chemical composition quality of raw tobacco packs purchased and stored by tobacco leaf and tobacco enterprises, it is difficult to realize the detection of multi-point samples, but only a few samples are taken from each large frame (a basket of tobacco contains several packs of tobacco leaves). The leaves represent the quality of the whole frame of tobacco leaves, which also objectively magnifies the random error of sampling

Method used

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  • Method for improving detection efficiency and representativeness of chemical components of crude tobacco package
  • Method for improving detection efficiency and representativeness of chemical components of crude tobacco package
  • Method for improving detection efficiency and representativeness of chemical components of crude tobacco package

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0049] S1: Take four times of multi-point sampling on the four corners of the original cigarette pack of No. 1 cigarettes and sample 3 tobacco leaves each time, and mix the obtained tobacco leaves for a total of 12 pieces for inspection;

[0050] S2: Lay the tobacco leaves obtained in s1 on the detection conveyor belt, start the detection conveyor belt, and the tobacco leaves are conveyed by the detection conveyor belt for 60s through the spot irradiation detection area of ​​the online near infrared spectrometer, and the detection value is recorded;

[0051] S3: Perform numerical averaging optimization processing on the numerical value obtained in S2 to obtain the chemical composition value of the entire pack of the original cigarette pack. See the table below:

[0052] Sample serial number 7440 near infrared (%) Laboratory test value (%) deviation(%) number 14.214.330.12

Embodiment 2

[0054] S1: Take five multi-point sampling of the four corners of the original cigarette pack and the tobacco leaves in the middle of the pack of No. 1 original cigarettes, and sample 2 tobacco leaves each time, and mix together 15 pieces of tobacco leaves to be inspected;

[0055] S2: Lay the tobacco leaves obtained in s1 on the detection conveyor belt, start the detection conveyor belt, and the tobacco leaves are conveyed by the detection conveyor belt for 20s through the light spot of the online near-infrared spectrometer to illuminate the detection area, and the detection value is recorded;

[0056] S3: Perform numerical averaging optimization processing on the numerical value obtained in S2 to obtain the chemical composition value of the entire pack of the original cigarette pack. See the table below:

[0057] Sample serial number 7440 near infrared (%) Laboratory test value (%) deviation(%) number 14.264.330.07

Embodiment 3

[0059] S1: Perform the S-type sampling method on the original cigarette pack of No. 1 tested and sample 15 tobacco leaves and mix them for inspection;

[0060] S2, spread the tobacco leaves obtained in s1 on the detection conveyor belt, and the tobacco leaves are conveyed by the detection conveyor belt for 120s through the spot of the online near infrared spectrometer to irradiate the detection area, and the detection value is recorded;

[0061] S3: Perform numerical averaging optimization processing on the numerical value obtained in S2 to obtain the chemical composition value of the entire pack of the original cigarette pack. See the table below:

[0062] Sample serial number 7440 near infrared (%) Laboratory test value (%) deviation(%) number 14.304.330.03

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Abstract

The invention relates to a method for improving mass detection of chemical components of a crude tobacco package in tobacco leaf tobacco industries, and in particularly relates to a method for improving the detection efficiency and representativeness of the chemical components of the crude tobacco package. The method includes the following steps: sampling multiple points of tobacco leaves in a to-be-tested crude tobacco package for four or more than times, and mixing the tobacco leaves obtained by the four or more than times of sampling for detecting; spreading flatly the obtained tobacco leaves on a detection conveyor belt, starting the detection conveyor belt, conveying the tobacco leaves by the detection conveyor belt to pass through a light spot irradiation detection area of an on-line near infrared spectroscopy, processing obtained near infrared spectrum of each chemical component by detecting measuring software for detecting, and after the processing by the detecting measuring software, outputting detection numerical values of all the chemical components, and recording the numerical values of all the chemical components; performing numerical optimization on the numerical values obtained by the on-line near infrared spectroscopy to obtain the chemical component values of the whole crude tobacco package. The fast detection function of the chemical components of the crude tobacco hemp package can be realized, and the method has the advantage of high efficiency, complete detection and representative detection values.

Description

Technical field [0001] The invention relates to a method for inspecting the quality of chemical components of original tobacco packets in the tobacco industry, in particular to a method for improving the detection efficiency and representativeness of the chemical components of original tobacco packets. Background technique [0002] In order to facilitate the handling of original cigarette packs, tobacco companies often carry out the processing of about several large baskets of cigarette packs. When conducting random inspections on the chemical composition of raw cigarettes, they only take them from each large frame. A small number of leaves undergo offline chemical composition testing to represent the quality of the whole frame of tobacco leaves. The test result of a randomly selected sample represents the chemical quality of a pack or several packs of tobacco leaves, which is neither representative nor reflective of the true situation, and objectively amplifies the random error ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/359
CPCG01N21/359
Inventor 张俊荣崔建军唐天宽刘洪标刘华友唐春平胡孟易萍艳黄小艳张智勇秦颖飞云川钱瑜蒋明民倪勇
Owner YUNNAN KUNMING SHIPBUILDING DESIGN & RESEARCH INSTITUTE
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