Method for preparing polycarboxylic acid anti-sloughing agent
A technology of slump-preserving agent and polycarboxylic acid, which is applied in the field of concrete admixture, can solve the problems of polycarboxylate superplasticizer with weak slump-preserving ability, prolonged concrete setting time, and failure to meet engineering needs, etc., achieving obvious slump-preserving effect, Overcoming the effect of low early strength and increased strength
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[0012] As a kind of embodiment of the present invention, a kind of method for preparing polycarboxylate anti-slump agent, comprises the following steps:
[0013] In the first step, according to 7% isoprenyl polyoxyethylene ether, 5.5% maleic anhydride, 16% ammonium acrylamide, 4.5% hydroxypropyl acrylate, 8.5% sodium methacrylate, and 3.7% sodium hydroxide %, the balance is the weight ratio of water. Prepare each component and put each component in a container. Take a part of water from the water container and add it to the reactor and heat the water in the reactor to 46-50°C, then add isoprenyl polyoxyethylene ether into the reaction kettle while stirring;
[0014] In the second step, after the isoprenyl polyoxyethylene ether is completely dissolved, add maleic anhydride, ammonium acrylamide, hydroxypropyl acrylate, and sodium methacrylene sulfonate successively to the reaction kettle, and continuously stir for 4- 4.5 hours;
[0015] In the third step, sodium hydroxide and ...
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