Synthetic method of 2,5-furandimethanol and its etherification product
A technology of furandimethanol and a synthesis method, which is applied in the field of synthesis of 2,5-furandimethanol and its etherification products, can solve the problems of difficulty in obtaining raw materials, high cost and high catalyst cost, and achieves good reusability and reaction system. Simple and economical results
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Embodiment 1~5
[0025] Add 0.4g 5-hydroxymethylfurfural and 19.6g isopropanol (2wt%) in the autoclave of 50mL, then add 0.2gZrO 2 / MCM-41, ZrO 2 / Beta1401, ZrO 2 / USY, ZrO 2 / SBA-15(ZrO 2 The loading capacity is 40%) as a catalyst, seal the reactor, stir vigorously (500rpm), heat to 150°C and keep for 2.5h, finish the reaction and cool to room temperature and take samples, use GC-MS (Shimadzu) and GC (Agilent) Qualitative and quantitative tests were carried out, and the test results are listed in Table 1, numbered 1-5.
Embodiment 6
[0027] Add 0.4g 5-hydroxymethylfurfural and 19.6g isopropanol (2wt%) in the autoclave of 50mL, then add 0.2gZrO 2 / SBA-15(ZrO 2 The loading amount is 40wt%) as a catalyst, seal the reactor, vigorously stir (500rpm), heat to 150 ° C and keep for 4h, finish the reaction and cool to room temperature and take samples, use GC-MS (Shimadzu) and GC (Agilent) to carry out Qualitative and quantitative detection, the detection results are listed in Table 1, the serial number is 6.
Embodiment 7~10
[0029] Add 0.4g 5-hydroxymethylfurfural and 19.6g methanol (2wt%) in the 50mL autoclave, then add 0.2gMgO-ZrO 2 / SBA-15,K 2 O-ZrO 2 / SBA-15, CaO-ZrO 2 / SBA-15, BaO-ZrO 2 / SBA-15 (the load of metal oxide is 40wt%, the mixing ratio of the two metal oxides is 1:1) as a catalyst, seal the reactor, stir vigorously (500rpm), heat to 100°C and keep it for 2.5h, After finishing the reaction, cool down to room temperature and take samples. GC-MS (Shimadzu) and GC (Agilent) are used for qualitative and quantitative detection. The detection results of different catalysts are listed in Table 1, numbered 7-10.
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