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Controllable capsule gel breaker and preparation method thereof

A capsule gel breaker and capsule coating technology, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of uncontrollable gel breaking time, single gel breaking time, and affecting normal work, etc., and achieve long-term maintenance No release, strong gel breaking ability, and strong stability

Active Publication Date: 2021-02-19
北京科美润能源科技发展有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] At present, although some capsule gel breakers on the market can play the role of delaying the release of gel breakers, their gel breaking time is uncontrollable, and there are cases of premature or too late gel breaking, which affects normal work
The Chinese patent with the notification number CN102627959B discloses a microcapsule breaker that can be controlled and released within 2 to 3 hours. need
At the same time, the inventors have found that the microcapsule breaker is only suitable for normal temperature, and if the temperature is too high, the microcapsule breaker will fail

Method used

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  • Controllable capsule gel breaker and preparation method thereof
  • Controllable capsule gel breaker and preparation method thereof
  • Controllable capsule gel breaker and preparation method thereof

Examples

Experimental program
Comparison scheme
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Embodiment 1

[0039] Take sulfate, biological enzyme, and alkylsulfonate, and sieve them through a 100-mesh sieve respectively. Take 400 parts of sieved sulfate, 300 parts of sieved biological enzyme and 100 parts of sifted alkylsulfonate, mix them evenly, and pass through a 100-mesh sieve. Put the mixture into a granulator, add 300 parts of mixed resin binder, and add water to dilute by 1 time. Stir evenly, adjust the pH to 5-8, and wet granulate at 20-60°C to make granules. The particles are dried at 30-60° C. for 2-10 hours, passed through a 40-14 mesh sieve, and uniformly dispersed to obtain a capsule core.

[0040] Take polyamide and epoxy resin, and pass through 100 mesh sieves respectively. Take 100 parts of sieved polyamide and 300 parts of sieved epoxy resin, mix them evenly, and pass through a 100-mesh sieve. The mixture of polyamide and epoxy resin is sprayed onto the capsule core by gas suspension in a fluidized bed, and dried at 30-60° C. for 2-10 hours to obtain a capsule c...

Embodiment 2

[0043] Take fluoride salt, bacillus, and alkylbenzene sulfonate, and sieve through 100 meshes respectively. Take 500 parts of sifted fluoride salt, 300 parts of sifted bacillus and 200 parts of sifted alkylbenzene sulfonate, mix them evenly, and pass through a 100-mesh sieve. Put the mixture into a granulator, add 200 parts of mixed resin binder, and add water to dilute 0.8 times. Stir evenly, adjust the pH to 5-8, and wet granulate at 20-60°C to make granules. The particles are dried at 30-60° C. for 2-10 hours, passed through a 40-14 mesh sieve, and uniformly dispersed to obtain a capsule core.

[0044] Take polyamide and epoxy resin, and pass through 100 mesh sieves respectively. Take 200 parts of sieved polyamide and 150 parts of sieved epoxy resin, mix them evenly, and pass through a 100-mesh sieve. The mixture of polyamide and epoxy resin is sprayed onto the capsule core by gas suspension in a fluidized bed, and dried at 30-60° C. for 2-10 hours to obtain a capsule co...

Embodiment 3

[0047] Take fluoroborate, biological enzyme, bacillus, and alkyl sulfate salt, and sieve through 100 meshes respectively. Take 100 parts of sifted fluoroborate, 100 parts of sifted biological enzyme, 100 parts of sifted bacillus and 100 parts of sifted alkyl sulfate salt, mix them evenly, and pass through a 100-mesh sieve. Put the mixture into a granulator, add 100 parts of epoxy resin binder, and add water to dilute 0.5 times. Stir evenly, adjust the pH to 5-8, and wet granulate at 20-60°C to make granules. The particles are dried at 30-60° C. for 2-10 hours, passed through a 40-14 mesh sieve, and uniformly dispersed to obtain a capsule core.

[0048] Take the modified aromatic amine and epoxy resin, and pass through a 100-mesh sieve respectively. Take 100 parts of sieved modified aromatic amine and 50 parts of sieved epoxy resin, mix them evenly, and pass through a 100-mesh sieve. The mixture of modified aromatic amine and epoxy resin is sprayed onto the capsule core by g...

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Abstract

The invention discloses a controllable capsule gel breaker and a preparation method thereof. The controllable capsule gel breaker is prepared from the following raw materials in parts by weight as main components: 300-1000 parts of active ingredients, adhesive 20-300 parts, 50-600 parts of temperature-resistant micro-permeable inner capsule, 50-600 parts of temperature-resistant and waterproof polymer outer capsule. The controllable capsule gel breaker uses active ingredients and a binder as the capsule core, and is sequentially sprayed with a temperature-resistant micro-permeable inner capsule coat and a temperature-resistant waterproof polymer outer capsule coat. The purpose of the present invention is to provide a controllable capsule gel breaker suitable for various gel breaking objects, suitable for gel breaking temperature of 0-120°C, controllable gel breaking time and strong gel breaking ability and its preparation method.

Description

technical field [0001] The invention relates to a gel breaker, more specifically, it relates to a controllable capsule gel breaker and a preparation method thereof. Background technique [0002] Gel breakers are widely used in the industrial field, such as the breaking of fracturing fluid in the petroleum industry and [0003] Capsule gel breaker is a new type of gel breaker that has developed rapidly in recent years. It is coated with a capsule coat on the gel breaker. The principle of the capsule gel breaker is that the capsule coat is broken under a certain extrusion force or soaked in high temperature for a long time, and the gel breaker is released. The capsule gel breaker has the characteristic of delayed release. [0004] At present, although some capsule gel breakers on the market can delay the release of gel breakers, their gel breaking time is uncontrollable, and there are cases of premature or too late gel breaking, which affects normal work. The Chinese patent ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K8/70
CPCC09K8/706C09K2208/24C09K2208/26
Inventor 刘文静
Owner 北京科美润能源科技发展有限公司