Method for preparing a hand washing liquid from periploca sepium bunge
A hand sanitizer and bar willow technology, which is applied in the field of hand sanitizer preparation, can solve the problems of hand skin damage, increase production cost, excessive use, etc., and achieve the effect of light fragrance, good moisturizing type and low price
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Embodiment 1
[0019] A method for preparing hand sanitizer by using bar willows, comprising the following steps:
[0020] (1) chop up the aboveground vegetative body of the willow bark and dry it, add 8 times the weight of 75% ethanol solution to heat and reflux for extraction, and concentrate the extract to 40% of the original volume to obtain a thick paste-like substance;
[0021] (2) Add a sufficient amount of hydrochloric acid with a volume fraction of 20% to the prepared thick paste to dissolve it into a transparent solution, then add a sodium bicarbonate solution with a volume fraction of 10% to it, and heat slowly Stir continuously at 80°C, and after 5 minutes of heat preservation, centrifuge the mixture to obtain the centrifuged supernatant;
[0022] (3) Add 1.5 times the volume of mixed alcohol to the prepared centrifuge supernatant, raise the temperature of the mixture to 40°C, and keep it warm for 3 hours to obtain the active component of hand sanitizer, wherein the mixed alcohol...
Embodiment 2
[0029] A method for preparing hand sanitizer by using bar willows, comprising the following steps:
[0030] (1) chop up the aboveground vegetative body of the willow bark and dry it, add 9 times the weight of 75% ethanol solution to heat and reflux for extraction, and concentrate the extract to 45% of the original volume to obtain a thick paste-like substance;
[0031] (2) Add a sufficient amount of hydrochloric acid with a volume fraction of 25% to the prepared thick paste to dissolve it into a transparent solution, then add a sodium bicarbonate solution with a volume fraction of 13%, and heat slowly Stir continuously at 80°C, and after 7 minutes of incubation, centrifuge the mixture to obtain the centrifuged supernatant;
[0032] (3) Add 2.0 times the volume of mixed alcohol to the prepared centrifuge supernatant, raise the temperature of the mixture to 50°C, and keep it warm for 4 hours to obtain the active component of hand sanitizer, wherein the mixed alcohol consists of ...
Embodiment 3
[0039] A method for preparing hand sanitizer by using bar willows, comprising the following steps:
[0040] (1) chop up the aboveground vegetative bodies of the willow bark and dry them, add 10 times the weight of 75% ethanol solution to heat and reflux for extraction, and concentrate the extract to 50% of the original volume to obtain a thick paste-like substance;
[0041] (2) Add a sufficient amount of hydrochloric acid with a volume fraction of 30% to the prepared thick paste to dissolve it into a transparent solution, then add a sodium bicarbonate solution with a volume fraction of 15% to it, and heat slowly Stir continuously at 80°C, and after 10 minutes of heat preservation, centrifuge the mixture to obtain the centrifuged supernatant;
[0042] (3) Add 2.5 times the volume of mixed alcohol to the prepared centrifuge supernatant, raise the temperature of the mixture to 55°C, and keep it warm for 5 hours to obtain the active component of hand sanitizer, wherein the mixed a...
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